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Pigment dispersing agent prepared by amphiphilic precipitated silica

A technology for precipitating silica and pigment dispersants, applied in the field of pigment dispersants, can solve the problems of inability to achieve long-term dispersion and suspension of pigment particles, poor dispersant stability, pigment sedimentation, etc., to avoid pigment flocculation, ensure the effect of painting, The effect of enhancing fluidity and thermal stability

Active Publication Date: 2017-02-08
ANHUI LONGQUAN SILICON MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the stability of the currently used dispersant is poor, and it cannot meet the requirement of long-term dispersion and suspension of the pigment particles in the paint base. During the storage of the paint, the phenomenon of pigment sedimentation and precipitation will occur. Therefore, it is urgent to develop a new type of pigment dispersant.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] (1) Add 5 parts of terpene resin and 3 parts of microcrystalline wax to 15 parts of amphiphilic precipitated silica, first heat to 90-100°C and mix for 5 minutes, then add 4 parts of hydrogenated castor oil and 1 part of nano rubber powder , continue to heat to 120-130 ° C and mix for 10 minutes to obtain material I;

[0019] (2) Add 6 parts of cetyl ethylhexanoate and 1 part of isooctyl oleate to 10 parts of isopropanol, heat it to reflux state for 10 minutes while stirring, then add 2 parts of turpentine and 1 part of titanic acid Ester coupling agent and 1 part of vulcanized lard, continue to reflux and keep stirring for 10 minutes to obtain material II;

[0020] (3) Add material I, 3 parts of polyethylene glycol 400 and 3 parts of sodium polyacrylate to material II, mix thoroughly and then microwave at microwave frequency 2450MHz and power 700W for 10min, and finally cool the mixture to 60-65 After ℃, add 5 parts of polyvinylpyrrolidone, 3 parts of sodium cocoyl gl...

Embodiment 2

[0023] (1) Add 5 parts of terpene resin and 4 parts of microcrystalline wax to 20 parts of amphiphilic precipitated silica, first heat to 90-100 ° C and mix for 5 minutes, then add 5 parts of hydrogenated castor oil and 0.5 parts of nano rubber powder , continue to heat to 120-130 ° C and mix for 10 minutes to obtain material I;

[0024] (2) Add 6 parts of cetyl ethylhexanoate and 2 parts of isooctyl oleate to 15 parts of isopropanol, heat it to reflux state for 10 minutes while stirring, then add 2 parts of turpentine and 1 part of titanic acid Ester coupling agent and 0.5 part of vulcanized lard, continue to reflux and keep stirring for 10 minutes to obtain material II;

[0025] (3) Add material I, 5 parts of polyethylene glycol 400 and 2 parts of sodium polyacrylate to material II, mix thoroughly and microwave at microwave frequency 2450MHz, power 700W for 10min, and finally wait for the temperature of the mixture to cool naturally to 60-65 After ℃, add 6 parts of polyviny...

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PUM

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Abstract

The invention discloses a pigment dispersing agent prepared by the amphiphilic precipitated silica and relates to the technical field of precipitated silica. The pigment dispersing agent is prepared from the following raw materials in parts by weight: 15-20 parts of amphiphilic precipitated silica, 10-15 parts of isopropyl alcohol, 6-11 parts of cetyl ethyl hexanoate, 5-9 parts of terpene resin, 5-9 parts of polyvinylpyrrolidone, 4-7 parts of hydrogenated castor oil, 3-6 parts of microcrystalline wax, 3-6 parts of polyethylene glycol 400, 2-4 parts of sodium cocoanutylglutamate, 2-4 parts of sodium polyacrylate, 2-4 parts of turpentine oil, 1-2 parts of isooctyl oleate, 1-2 parts of coupling agent of organic titanate, 0.5-1 part of nano gelatine powders, 0.5-1 part of urea, and 0.5-1 part of sulfurized lard oil. According to the invention, by means of the pigment dispersing agent, the pigment is uniformly dispersed in a binder, so that the particles of the pigment are uniformly suspended in the binder for a long time. Therefore, during the storage process of a colored paint, the pigment flocculation phenomenon is avoided. Moreover, the fluidity and the thermal stability of the colored paint are improved, so that the storage quality and the painting effect of the colored paint can be ensured.

Description

[0001] Technical field: [0002] The invention relates to the technical field of precipitated silica, in particular to a pigment dispersant prepared by using amphiphilic precipitated silica. [0003] Background technique: [0004] In addition to the wetting effect of the wetting agent, the pigment dispersant has one end of the active group that can be adsorbed on the surface of the pigment that is crushed into fine particles, and the other end is solvated into the paint base to form an adsorption layer, resulting in charge repulsion or entropy repulsion. The pigment particles are dispersed and suspended in the paint base for a long time to avoid re-flocculation, thus ensuring the storage stability of the prepared color paint system. However, the stability of the currently used dispersant is poor, and it cannot meet the requirement of long-term dispersion and suspension of pigment particles in the paint base. During the storage of the paint, the phenomenon of pigment sedimentati...

Claims

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Application Information

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IPC IPC(8): B01F17/54C09D7/12C09K23/54
CPCC09K23/002
Inventor 赵东旭汪树龙董珂连佩兵沈颂良
Owner ANHUI LONGQUAN SILICON MATERIAL
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