Preparation method of MgO-doped ZnO sputtering target material
A sputtering target and target technology, applied in sputtering coating, metal material coating process, ion implantation coating and other directions, can solve the problems of high requirements, complicated preparation process and difficult to control, expensive equipment, etc. Good dispersion, excellent luminous properties, uniform particle effect
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[0020] In the present invention, the preparation method steps include:
[0021] (1) Weigh ZnO and MgO powders in proportion, the powder purity is greater than 99.99%, and put the two powders into a nylon ball mill jar.
[0022] (2) Add absolute ethanol and agate balls of different diameters into the ball mill jar, the weight ratio of ZnO and MgO powder, agate balls and absolute ethanol is 10:16:20.
[0023] (3) Put ZnO powder, MgO powder, absolute ethanol and agate balls into a nylon tank and place them on a star ball mill to fix them.
[0024] (4) After quick ball milling for 2 hours, take out the mixed powder in the nylon tank, and separate the agate balls through a 40-mesh sieve.
[0025] (5) Put the uniformly mixed ZnO powder and MgO powder into a low-temperature oven and dry with absolute ethanol.
[0026] (6) The dried ZnO powder and MgO powder are filled into a high temperature resistant and pressure resistant mold.
[0027] (7) Put the mold in a heated and pressuriz...
Embodiment 1
[0032] Weigh 500 g of ZnO powder with a purity of 99.99% and 20 g of MgO powder with a purity of 99.99%, put it into a nylon ball mill jar with a volume of 5 L, and then put into 800 g of agate balls and 1 kg of absolute ethanol. The nylon ball mill jar was fixed on a high-speed ball mill and ball milled for 3 hours. Use a 40-mesh sieve to separate the agate balls. The powder solution separated with a sieve is placed in a baking tray, and the baking tray is put into an oven and baked for 4 hours at a temperature of 60°C. The dried powder is packed in a 1800°C-resistant mold with a size of 200mm×200mm×500mm. The mold is placed in a heating and pressurizing furnace filled with an oxidizing atmosphere. The heating rate of the furnace is 15°C / min, and the maximum temperature is 1200°C for 3 hours. . Pressurize at a speed of 0.2MPa, to a maximum pressure of 15MPa, and keep pressurized for 5 hours; cool down in the furnace, and after the heat preservation and pressure holding are ...
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