A kind of environment-friendly toughening adhesive for recombined decorative materials and its application
A technology for reorganizing decorative materials and adhesives, applied in the directions of adhesives, adhesive types, starch adhesives, etc., can solve the problems of poor toughness, low environmental protection, low formaldehyde emission, etc., to improve environmental protection and toughness. , The effect of high environmental protection
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Embodiment 1
[0028] a. Preparation of modified micro-nano cellulose: the wood or straw fibers from which lignin and hemicellulose have been removed are stirred and reacted with an acid solution with a mass fraction of 45% at 60°C for 2 hours to form a cellulose slurry. The cellulose slurry was added with water to adjust the concentration to 1.8%, and then the cellulose slurry was subjected to low-temperature ultrasonic pretreatment at 8° C., ultrasonic power of 650 W, and ultrasonic frequency of 20 kHz for 40 minutes, and then the cellulose slurry was subjected to high pressure at 100 MPa. The homogenization cycle is 6 times, and then the cellulose slurry is added with water to adjust the concentration to 1.5%, and then 2% of the cellulose slurry mass is added with a silane coupling agent and at 40°C, nitrogen gas flow rate 18ml / min After exhausting oxygen for 7 minutes, perform an in-situ ultrasonic reaction at an ultrasonic power of 750 W and an ultrasonic frequency of 20 kHz for 18 minut...
Embodiment 2
[0035] a. Preparation of modified micro / nano cellulose: the wood or straw fibers from which lignin and hemicellulose have been removed are stirred and reacted with an acid solution of 30% by mass at 40°C for 3 hours to form a cellulose slurry. Add water to the cellulose slurry to adjust the concentration to 1.5%, and then pretreat the cellulose slurry with low-temperature ultrasound at 10°C, ultrasonic power of 1000 W, and ultrasonic frequency of 22 kHz for 60 minutes, and then subject the cellulose slurry to high pressure at 120 MPa The homogenization cycle is 7 times, and then the cellulose slurry is added with water to adjust the concentration to 1%, and then 2% of the cellulose slurry mass is added with a silane coupling agent and the airflow rate is 30ml / min at 40℃ and nitrogen. After exhausting oxygen for 3 minutes, an in-situ ultrasonic reaction was performed at an ultrasonic power of 900 W and an ultrasonic frequency of 18 kHz for 20 minutes to prepare the modified micr...
Embodiment 3
[0042] a. Preparation of modified micro / nano cellulose: the wood or straw fibers from which lignin and hemicellulose have been removed are stirred and reacted with an acid solution with a mass fraction of 60% at 80°C for 1 hour to form a cellulose slurry. The cellulose slurry was added with water to adjust the concentration to 1.8%, and then the cellulose slurry was pretreated by low-temperature ultrasound at 5°C, ultrasonic power of 1000W, and ultrasonic frequency of 22kHz for 30 minutes, and then the cellulose slurry was subjected to high pressure at 150MPa Homogenize twice, then add water to the cellulose slurry to adjust the concentration to 2%, then add 3% of the cellulose slurry mass of the silane coupling agent and at 30°C, nitrogen gas flow rate 5ml / min After exhausting oxygen for 10 minutes, perform an in-situ ultrasonic reaction for 30 minutes at an ultrasonic power of 600W and an ultrasonic frequency of 22kHz to prepare the modified micro-nanocellulose; the silane co...
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