Scanning electron microscopy sample production method of coated white cardboard fracture

A technology of scanning electron microscopy and white paperboard, which is applied in the preparation of test samples, etc., can solve the problem of affecting the observation effect of scanning electron microscopy on the surface coating of paper, it is difficult to obtain a flat fracture, and the difference in mechanical properties between inorganic coating and core fiber is relatively large. Large and other problems, to achieve the effect of simple and fast sample preparation method, no pollutant blocking, and good application prospects

Inactive Publication Date: 2017-02-22
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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Problems solved by technology

However, when cutting directly with scissors, due to the large difference in mechanical properties between the inorganic coating and the core fiber, it is difficult to obtain a flat fracture that meets the scanning electron microscope observation
Using the metallographic polishing method, the residual polishing material is easy to form pollutants, which affects the scanning electron microscope observation effect of the paper surface coating

Method used

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  • Scanning electron microscopy sample production method of coated white cardboard fracture
  • Scanning electron microscopy sample production method of coated white cardboard fracture
  • Scanning electron microscopy sample production method of coated white cardboard fracture

Examples

Experimental program
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Embodiment

[0030] Function in this example embodiment, coated white cardboard thickness is 0.3mm, and cardboard surface is double-layer calcium carbonate coating, and the scanning electron microscope sample preparation method of its fracture is as follows:

[0031] (1) if figure 1 As shown, use scissors to cut the coated white cardboard into a strip sample with a width of 10mm and a length of 20mm, and then trim one end of the strip sample along the length direction into a pointed shape with a length of 5mm and a thickness of 0.3mm, and the width of the tip is 2mm;

[0032] (2) Fix the tip of the sample upwards on the sample stage of a mechanical pusher ultramicrotome equipped with a microscope; adjust the magnification of the microscope to 4.6 times, and use a blade to modify the tip of the sample under the microscope, and trim the width of the tip to About 1mm; then adjust the magnification of the microscope to 20 times, continue to modify the tip with a blade, and finally trim the ti...

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Abstract

The invention provides a scanning electron microscopy sample production method of a coated white cardboard fracture. The method comprises the following steps: shearing a coated white cardboard to form a long strip, wherein one end of the long strip along the length direction is sharp-pointed, and the width of the tip is less than or equal to 0.5 mm; and slicing the tip of the long strip through adopting a mechanically propelled ultrathin slicing machine by using a diamond cutter at a slicing rate of below 0.5 mm/sec in order to obtain the coated white cardboard fracture. The coated white cardboard fracture produced by using the method is clean and flat without pollutant shielding, so the clear coated white cardboard fracture microscopic picture of the sample fracture is obtained, and analysis test of the thickness of a white cardboard coating and the particle size and the shape of particles is realized by using a scanning electron microscope.

Description

technical field [0001] The invention relates to a scanning electron microscope sample preparation method, in particular to a scanning electron microscope sample preparation method for coating the fracture of a white paperboard. Background technique [0002] White cardboard is a kind of cardboard with a smooth and white front and a smoother back. Coated white paperboard refers to the processed paperboard made by coating and finishing the surface of the original paperboard, and its weight is generally 200g / m 2 up to 400g / m 2 between. The whiteness, smoothness, glossiness and surface strength of the coated white paperboard are good, and it has good strength performance, so it is suitable for high-speed color printing and can meet the packaging requirements. It has become one of the most widely consumed paper types in my country. [0003] White cardboard is composed of surface layer, core board and bottom layer. The core layer of white cardboard is generally made of mechanic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28
Inventor 陈国新卢焕明刘艳李明魏艳萍孙可卿
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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