Method for extracting rose essential oil by molecular sieve extracting agent
A technology of rose essential oil and molecular sieve, which is applied in the direction of essential oil/fragrance, fat production, etc. It can solve the problems of high distillation temperature, low oil yield, transformation and deterioration of active aroma components, achieve pure and bright color, and improve wetting performance , Fragrant and strong effect
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Embodiment 1
[0024] A method for extracting rose essential oil with a molecular sieve extractant, prepared through the following steps:
[0025] Clean the fresh rose petals that are not fully open and cut off the receptacle, dry naturally, stir in a blender for 4 minutes to form flower sauce, weigh 1000g flower sauce, 1000g 1.5% mesoporous molecular sieve and dodecylbenzenesulfonic acid An aqueous solution of sodium (the mass ratio of the two is 1:2) was added to a 5000ml three-necked bottle. Heat up to 40°C, stir for 1h, filter under reduced pressure, collect the filtrate, transfer it to a 5000ml distillation flask, steam distill, the distillate is a mixture of essential oil and water, use an oil-water separator to separate and remove water, and obtain 0.21g of an oily liquid product with color, clear and transparent, and pure aroma.
Embodiment 2
[0027] A method for extracting rose essential oil with a molecular sieve extractant, prepared through the following steps:
[0028] Wash the rose petals that are not fully opened and cut off the receptacle, dry naturally, and stir in a blender for 4 minutes to form a flower sauce. Weigh 1000g flower sauce, 1000g aqueous solution of 1.5% mesoporous molecular sieve and sodium dodecylbenzenesulfonate (the mass ratio of the two is 1:2.5), and add them into a 5000ml three-necked bottle. Heat up to 40°C and stir for 1h. Filtrate under reduced pressure, collect filtrate, it is transferred in the distillation flask of 5000ml, steam distillation, distillate is the mixture of essential oil and water. Separate the water with an oil-water separator to obtain 0.20 g of a colorless, clear and transparent oily liquid product with pure aroma.
Embodiment 3
[0030] A method for extracting rose essential oil with a molecular sieve extractant, prepared through the following steps:
[0031] Wash the rose petals that are not fully opened and cut off the receptacle, dry naturally, and stir in a blender for 4 minutes to form a flower sauce. Weigh 1000g flower sauce, 1000g aqueous solution of 1.5% mesoporous molecular sieve and sodium dodecylbenzenesulfonate (the mass ratio of the two is 1:3), and add them into a 5000ml three-necked bottle. Heat up to 40°C and stir for 1h. Filtrate under reduced pressure, collect filtrate, it is transferred in the distillation flask of 5000ml, steam distillation, distillate is the mixture of essential oil and water. Separate the water with an oil-water separator to obtain 0.20 g of a colorless, clear and transparent oily liquid product with pure aroma.
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