Phosphaphenanthrene triazine double-radical compound attached fire-retardant fibers and preparation method thereof
A technology of flame retardant fibers and compounds, applied in the directions of flame retardant fibers, fiber processing, textiles and papermaking, etc., can solve the problems of poor stability and compatibility, general flame retardant effect, and limited application of polyester fabrics. Excellent processing performance, low combustion toxicity, convenient for industrial production
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Embodiment 1
[0037] Put 5g of TAIC-DOPO, 50g of polyurethane resin, and 10g of toluene into a stirring pot, mix and stir evenly at 25°C to form a uniform coating glue, coat the coating glue on the fiber, and dry it at 150°C for 3 minutes. The LOI of the obtained flame-retardant fiber was 23.3%, and the tensile strength was 51.7 MPa.
Embodiment 2
[0039] Put 30g of TGIC-DOPO, 80g of polyurethane resin, and 15g of xylene into a stirring pot, mix and stir at 20°C for 0.1h to form a uniform coating glue, coat the coating glue on the fiber, and dry at 170°C After 2 minutes, the LOI of the obtained flame-retardant fiber was 23.9%, and the tensile strength was 52.7 MPa.
Embodiment 3
[0041] Put 8g of TAIC-DOPO, 70g of polyurethane resin, 12g of aluminum diethylphosphinate, and 12g of xylene into a stirring pot, mix and stir at 50°C for 0.3h to form a uniform coating glue, and coat the coating glue On the polyester fabric, drying at 180°C for 10 minutes, the LOI of the obtained flame-retardant polyester fabric is 26.7%, and the tensile strength is 54.2MPa.
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