Fragrant wool fiber and preparation method thereof
A technology of wool fiber and fragrance, which is applied in fiber treatment, animal fiber, textile and paper making, etc. It can solve the problems of large particle size, easy elution, and poor fragrance persistence, and achieve good biocompatibility, not easy elution, Long-lasting fragrance effect
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Embodiment 1
[0040] 1. Preparation method
[0041] Stir 5 g of Turkone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-buten-1-one) and 5 g of Tween Mix for 10 minutes to obtain Turkone emulsion; then add Turkone emulsion to 100mL 10wt% sodium tripolyphosphate aqueous solution, stir and mix for 10 minutes to obtain an oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate ; At a stirring speed of 500r / min, slowly add the oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate (O / W) into 100mL of 10wt% water-soluble chitosan aqueous solution, stir evenly, and react at room temperature for 2h. An aqueous solution of nanocapsules coated with Turkone was obtained.
[0042] Components by weight percent are 0.1wt% vanillin, 0.1wt% triethanolamine fatty acid ester quaternary ammonium salt, and the balance is water to prepare the aqueous solution of vanillin and triethanolamine fatty acid ester quaternary ammonium salt: vanillin and triethanolamine fatty acid ester quatern...
Embodiment 2
[0046] 1. Preparation method
[0047] Stir 5g Turkone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-buten-1-one) and 5g Span Mix for 10 minutes to obtain Turkone emulsion; then add Turkone emulsion to 100mL 10wt% sodium tripolyphosphate aqueous solution and stir and mix for 10 minutes to obtain an oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate; At a stirring speed of 600r / min, the oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate (O / W) was slowly added to 100mL of 10wt% water-soluble chitosan aqueous solution, stirred evenly, and reacted at room temperature for 2h to obtain An aqueous solution of nanocapsules coated with Turkone.
[0048]Component by weight percentage is 0.2wt% vanillin, 0.1wt% triethanolamine fatty acid ester quaternary ammonium salt, the balance is water, the aqueous solution of preparation vanillin and triethanolamine fatty acid ester quaternary ammonium salt: vanillin and triethanolamine fatty acid ester quaternary ...
Embodiment 3
[0052] 1. Preparation method
[0053] 10g Turkone ((E)-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-buten-1-one) and 10g polyethylene glycol Stir and mix with alcohol for 12 minutes to obtain Turkone emulsion; then add Turkone emulsion to 200mL 10wt% sodium tripolyphosphate aqueous solution and stir and mix for 12 minutes to obtain an oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate solution; at a stirring speed of 700r / min, slowly add the oil-in-water (O / W) mixture of Turkone and sodium tripolyphosphate (O / W) into 200mL of 10wt% water-soluble chitosan aqueous solution, stir evenly, and react at room temperature for 2h , to obtain an aqueous solution of nanocapsules coated with Turkone.
[0054] Components by weight percent are 0.4wt% vanillin, 0.2wt% triethanolamine fatty acid ester quaternary ammonium salt, and the balance is water to prepare the aqueous solution of vanillin and triethanolamine fatty acid ester quaternary ammonium salt: vanillin and trieth...
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