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559 results about "Sodium triphosphate" patented technology

Sodium triphosphate (STP), also sodium tripolyphosphate (STPP), or tripolyphosphate (TPP),) is an inorganic compound with formula Na₅P₃O₁₀. It is the sodium salt of the polyphosphate penta-anion, which is the conjugate base of triphosphoric acid. It is produced on a large scale as a component of many domestic and industrial products, especially detergents. Environmental problems associated with eutrophication are attributed to its widespread use.

Preparation method of fracture-resistant and wear-resistant ceramic

The invention belongs to the technical field of ceramics, and discloses a preparation method of fracture-resistant and wear-resistant ceramics. The preparation method comprises the following steps: weighing the raw materials in parts by weight; the preparation method comprises the following steps: mixing 40 parts of potassium feldspar, 10 to 25 parts of albite, 1 to 10 parts of kaolin, 1 to 10 parts of serpentine, 5 to 25 parts of dolomite, 2 to 9 parts of nano zirconium oxide, 0.1 to 1 part of nano cerium oxide, 0.1 to 1 part of nano molybdenum disulfide, 0.1 to 0.8 part of silicon carbide fiber, 0.5 to 2.5 parts of polyethylene glycol, 0.1 to 0.6 part of fullerene trifluoromethyl derivative, 0.1 to 3 parts of sodium dodecyl sulfate, 0.1 to 2 parts of sodium tripolyphosphate and 10 to 60 parts of solvent to obtain slurry; and carrying out spray granulation to obtain a blank, carrying out compression molding to obtain a green body, and sintering to obtain the fracture-resistant and wear-resistant ceramic. The breaking strength of the breaking-resistant and wear-resistant ceramic can exceed 70 MPa, and the length of a grinding pit does not exceed 8.5 mm.
Owner:GUANGDONG XINRUNCHENG CERAMICS

Mining inorganic environment-friendly reinforcing material and application thereof

The invention provides a mining inorganic environment-friendly reinforcing material and application thereof, and belongs to the technical field of mining reinforcing materials. A component A comprises the following components in parts by mass: 60-80 parts of anhydrite, 5-20 parts of lime, 5-10 parts of silica fume, 2-8 parts of sodium silicate, 1-0.5 part of a naphthalene water reducer, 3-7 parts of an early strength agent and 0.2-0.8 part of lithium salt; the component B comprises the following components in parts by mass: 50-70 parts of cement clinker, 10-30 parts of slag cement, 5-10 parts of iron powder, 1-8 parts of aluminum sulfate, 5-10 parts of calcium carbonate and 0.5-1 part of sodium tripolyphosphate; the component C is prepared from the following components in parts by mass: 10 to 25 parts of water glass, 10 to 20 parts of emulsion, 40 to 60 parts of water, 5 to 10 parts of high-efficiency water reducing agent and 1 to 5 parts of triethanolamine. The mining inorganic environment-friendly reinforcing material provided by the invention is low in reaction heat and is not easy to cause coal combustion.
Owner:SHANXI YUBANG NEW POWER SCI & TECH

Radiation refrigeration external wall brick and preparation process thereof

The invention discloses a radiation refrigeration exterior wall tile and a preparation process thereof, and relates to the technical field of ceramic tiles. The radiation refrigeration external wall tile comprises a green body, a ground coat layer, a pattern layer and a protective glaze layer from inside to outside, the ground glaze layer comprises the following components in parts by mass: 40-60 parts of ground glaze layer ceramic basic glaze, 15-35 parts of cooling powder, 6-12 parts of calcined talc, 4-8 parts of calcined zinc oxide, 3-6 parts of dolomite, 2-4 parts of fluorite, 3-6 parts of calcined kaolin, 0.2-0.5 part of sodium carboxymethyl cellulose, 0.2-0.5 part of sodium tripolyphosphate and 40-55 parts of clear water; the protective glaze layer comprises the following components in parts by mass: 60-70 parts of protective glaze layer ceramic basic glaze, 10-20 parts of cooling powder, 5-10 parts of albite, 3-5 parts of calcined talc, 2-4 parts of calcined zinc oxide, 0.2-0.5 part of sodium carboxymethyl cellulose, 0.2-0.5 part of sodium tripolyphosphate and 40-55 parts of clear water. By adjusting the component proportion of the ground coat layer and the protective glaze layer and adding the cooling powder for compounding, the basic performance of the wall brick can be ensured, and the reflection and radiance of the wall brick to infrared rays and visible light can be improved.
Owner:SHENZHEN CHUANGLENG TECH CO LTD

Wear-resistant and mildew-proof ceramic tile and preparation method thereof

The invention discloses a wear-resistant and mildew-proof ceramic tile which comprises a green body and a glaze layer attached to the green body, and the wear-resistant and mildew-proof ceramic tile is obtained by coating the surface of the green body with a modified interface agent and then glazing, wherein the glaze layer is prepared from the following raw materials in parts by weight: 40 to 50 parts of silicon dioxide, 30 to 35 parts of aluminum oxide, 15 to 20 parts of modified titanium dioxide, 6 to 10 parts of barium carbonate, 6 to 10 parts of mullite, 5 to 8 parts of silver-loaded zirconium phosphate, 4 to 8 parts of potassium carbonate, 4 to 8 parts of sodium carbonate, 3 to 7 parts of limestone, 3 to 5 parts of sodium borate, 2 to 4 parts of zinc oxide and 0.5 to 1 part of sodium tripolyphosphate. According to the ceramic tile, the modified interface agent with specific composition is introduced between the ceramic tile green body and the glaze layer, modified titanium dioxide and inorganic components (such as aluminum phosphate, aluminum acetylacetonate and tetrapropyl zirconate) in the interface agent form oxides in the sintering process, and the interface bonding strength is remarkably enhanced through physical occlusion; and the long-term wear resistance and mildew resistance of the ceramic tile glaze layer are improved.
Owner:FUJIAN SHANMEI NEW BUILDING MATERIALS CO LTD

Mulberry leaf flavone microcapsule as well as preparation method and application thereof

The invention relates to a mulberry leaf flavone microcapsule as well as a preparation method and application thereof, and belongs to the technical field of microcapsule drug loading. The preparation method of the mulberry leaf flavone microcapsule comprises the following steps: S1, adding mulberry leaf flavone into a chitosan solution, carrying out ultrasonic treatment, shearing by using a homogenizer, and heating and stirring to obtain a mixed solution; s2, slowly dropwise adding a sodium tripolyphosphate solution into the mixed solution, reacting and curing until the solution becomes milk white liquid from clear and no precipitate is generated, then centrifuging and washing, and collecting particles; and S3, freezing the particles, and performing freeze drying to obtain the mulberry leaf flavone microcapsules. The mulberry leaf flavone microcapsule provided by the invention can be used for developing a novel medicinal preparation in the field of medicines, and can relieve disease symptoms and delay disease progression through the antioxidant and anti-inflammatory characteristics of the mulberry leaf flavone microcapsule; in the field of food, the method can be applied to development of functional food, for example, the method can be added into beverages and health-care products to provide health benefits of antioxidation, blood fat reduction and the like for consumers.
Owner:HAINAN UNIV

GMT composite material automobile roof and preparation method thereof

The invention belongs to the technical field of automobile parts, and particularly discloses a GMT composite material automobile roof and a preparation method thereof. The GMT composite material automobile roof comprises a GMT composite board layer, a hot melt adhesive layer and a fabric layer, and is characterized in that the GMT composite board layer comprises the following components in parts by weight; comprising the following raw materials: 90-100 parts of composite fiber felt, 22-30 parts of modified bamboo fiber, 3-5 parts of tea tree oil, 1-2 parts of sodium tripolyphosphate, 2-4 parts of beta-glycerophosphate disodium, 0.5-0.8 part of lecithin, 15-20 parts of modified talcum powder, 4-6 parts of an expandable microsphere foaming agent and 190-200 parts of deionized water. The GMT composite material automobile ceiling prepared in the invention has excellent mechanical strength, durability and aging resistance, can provide mechanical protection for parts, and prolongs the service life of the automobile ceiling.
Owner:YANTAI ZHENGHAI HIGH TECH

Preparation method of nano-microspheres coated with nicotinamide mononucleotide shell membrane structure

The invention belongs to the field of nano preparations, and discloses a preparation method of nano microspheres coated with a nicotinamide mononucleotide shell membrane structure, which comprises the following steps: coating NMN in a pregel formed by chitosan and sodium tripolyphosphate, heating and stirring, adjusting the pH value to separate out chitosan-coated nano microspheres, drying to remove moisture on the surfaces of the nano microspheres, and drying to obtain the nano microspheres coated with the nicotinamide mononucleotide shell membrane structure. Then selecting a water phase and an oil phase in a proper proportion, preparing a chitosan / sodium alginate composite nano-microsphere with sodium alginate as an outer membrane by adopting an emulsion cross-linking method, and washing and drying to obtain the NMN nano-microsphere with a core-shell structure. According to the invention, NMN is coated in the nano-microsphere which is composed of two materials and has a nuclear membrane structure, so that the stability of NMN in a natural environment can be improved, hydrolysis of NMN by gastric acid and gastrointestinal tract enzyme in a drug delivery process can be prevented, the bioavailability of NMN is improved, and a drug sustained release effect is achieved.
Owner:DALIAN UNIV OF TECH +1

High-strength retarded magnesium phosphate cement as well as preparation method and application thereof

The invention provides high-strength retarded magnesium phosphate cement as well as a preparation method and application thereof, and belongs to the technical field of magnesium phosphate cement. The high-strength retarded magnesium phosphate cement provided by the invention is prepared from the following raw materials in parts by mass: 60 to 95 parts of dead burned magnesia powder, 20 to 50 parts of phosphate, 3 to 15 parts of a composite retarder, 5 to 20 parts of an admixture, 8 to 14 parts of fly ash microspheres, 1 to 2 parts of carbon nanotubes, 1 to 5 parts of carbon fibers and 5 to 30 parts of water, the composite retarder comprises sodium tripolyphosphate, zinc acetate, EDTA (Ethylene Diamine Tetraacetic Acid) disodium and polyacrylic acid; the admixture comprises phosphorus slag powder and silica fume. The result of the embodiment shows that the setting time of the high-strength delayed-setting magnesium phosphate cement provided by the invention is controllable between dozens of minutes and dozens of hours, meanwhile, the compressive strength of the magnesium phosphate cement 28d is greater than 90MPa, and the magnesium phosphate cement has excellent mechanical properties.
Owner:DALIAN UNIV OF TECH

Complex microbial inoculant, original cheese, processed cheese with function of reducing blood sugar and preparation and application of complex microbial inoculant

The invention belongs to the field of fermentation, and particularly relates to a complex microbial inoculant, original cheese, processed cheese with a blood sugar reducing function and preparation and application of the complex microbial inoculant. Wherein the processed cheese is prepared by the method comprising the following steps: mixing the components including raw cheese, sugarcane juice, corn oil, casein, concentrated milk protein, blueberry powder, mono / diglycerol fatty acid ester, sodium citrate, sodium tripolyphosphate, sodium hexametaphosphate, salt guar gum, potassium sorbate and water, and then emulsifying to obtain the processed cheese, the sugar cane juice, the corn oil, the casein, the concentrated milk protein, the blueberry powder, the mono / diglycerol fatty acid ester, the sodium citrate, the sodium tripolyphosphate, the sodium hexametaphosphate, the salt guar gum, the potassium sorbate and the water, the original cheese is prepared from a complex microbial inoculant, and the complex microbial inoculant comprises lactococcus lactis bacterial powder, lactococcus lactis subsp. Lactis bacterial powder, lactobacillus delbrueckii subsp. Lactis bacterial powder, lactobacillus plantarum bacterial powder and lactobacillus paracasei bacterial powder. The processed cheese provided by the invention has a better function of controlling blood sugar, and meanwhile, the processed cheese is fine and uniform in texture and has good smearing performance.
Owner:YICHANG XIWANG FOOD CO LTD +1

Refractory material containing waste magnesia-calcium bricks and preparation method thereof

The invention relates to the technical field of refractory materials, in particular to a waste magnesia-calcium brick-containing refractory material and a preparation method thereof, and the waste magnesia-calcium brick-containing refractory material comprises the following components: composite aggregate, calcium aluminate cement, urea resin-aluminum dihydrogen phosphate, active alpha-Al2O3 micro powder, silica micro powder and sodium tripolyphosphate. In the room-temperature spraying maintenance and low-temperature working stage, hydration of free CaO in the waste magnesia-calcium bricks and erosion of OH <-> are prevented through the hydrophobic effect of fluorinated polyphosphazene and modified zirconium oxide sol, and the compatibility and wettability of the composite aggregate and cement paste are improved through carboxylic acid groups of carboxyethyl silanetriol and polyethylene glycol monomethyl ether. According to the present invention, with the temperature rising, the aluminum dihydrogen phosphate forms the viscous liquid phase to wrap the aggregate so as to provide the temporary protection, the temperature continues to rise, the zirconium oxide and the nanometer Al2O3 react with the CaO and the MgO to generate the CaZrO3 and the MgAl2O3, the aluminum dihydrogen phosphate reacts with the nanometer Al2O3 in the system to generate the AlPO4, and the CaZrO3, the MgAl2O3 and the AlPO4 form the multi-phase fire-resistant structure so as to further improve the fire resistance of the fire-resistant material;
Owner:ZHONGMIN CHIYUAN IND

High-performance ceramic glaze for bacteriostatic domestic porcelain and preparation method of high-performance ceramic glaze

The invention relates to the technical field of glazes, and discloses a high-performance ceramic glaze for bacteriostatic domestic porcelain and a preparation method thereof. The high-performance ceramic glaze of the antibacterial domestic porcelain is prepared from the following raw materials in parts by weight: 5 to 15 parts of albite, 20 to 30 parts of potassium feldspar, 10 to 30 parts of kaolin, 13 to 26 parts of quartz, 0.3 to 7 parts of talc, 5 to 10 parts of limestone, 2 to 5 parts of ludwigite, 0.5 to 1 part of rare earth, 2 to 5 parts of honeysuckle-loaded CuS, 1 to 3 parts of modified polysiloxane, 0.1 to 0.5 part of sodium tripolyphosphate and 0.1 to 0.3 part of carboxymethyl cellulose. The high-performance ceramic glaze for the antibacterial domestic porcelain prepared by the invention has relatively good long-acting antibacterial performance and high strength.
Owner:GUANG DONG DA YE TAO CI YOU XIAN GONG SI +1

Chitosan nanocapsule as well as preparation method and application thereof

The invention relates to the technical field of functional materials, in particular to a chitosan nanocapsule as well as a preparation method and application thereof. The preparation method of the chitosan nanocapsule comprises the following steps: (a) mixing and emulsifying a chitosan solution, an oil-in-water emulsifier and essential oil to form an oil-in-water emulsion, adding an aqueous solution of sodium tripolyphosphate into the oil-in-water emulsion, and stirring to obtain a first mixture; (b) adding the first mixture into an oil phase solvent containing a water-in-oil emulsifier, and stirring to obtain a multiple emulsion; and (c) adding an aqueous solution of a dialdehyde cross-linking agent into the multiple emulsion, carrying out a cross-linking reaction, collecting a solid-phase substance, and drying. The physical / chemical double-crosslinking chitosan nanocapsule is obtained by utilizing physical crosslinking between the chitosan and the sodium tripolyphosphate and chemical crosslinking between the chitosan and the binary aldehyde crosslinking agent, so that the encapsulation efficiency and the encapsulation efficiency of the nanocapsule are remarkably improved; meanwhile, the nanocapsule also has pH responsiveness and has a slow release effect after pH response.
Owner:DONGHUA UNIV +1

Gel dressing for skin wound repair and preparation method thereof

The invention belongs to the technical field of bioengineering medicines, and particularly relates to a gel dressing for repairing skin wounds and a preparation method of the gel dressing. The anti-fouling coating is prepared from the following raw materials in parts by weight: 65 to 75 parts of polyvinyl alcohol, 14 to 20 parts of sodium alginate, 4 to 8 parts of sodium carboxymethyl cellulose, 1 to 3 parts of sodium hyaluronate, 12 to 22 parts of glycerol, 1 to 3 parts of surface anti-fouling additive, 6 to 10 parts of antibacterial microcapsule and 2 to 2.8 parts of compound ion. According to the invention, a PVA freeze-thaw physical network and an alginic acid Ca / Zn composite ion network cooperate to limit a pore channel, so that stable forming is realized; a chitosan / sodium tripolyphosphate microcapsule is prepared from polyhexamethylene biguanide hydrochloride and covered with sodium alginate, release sensitive to pH / ionic strength, acceleration in an inflammation stage and self-limiting in a later stage are constructed, and long-acting bacteriostasis is formed by SA-Zn site slow release; the stability and staged adaptation are highlighted through processes such as encapsulation, low-shear doping and the like and raw material synergy.
Owner:HANDAN RUIFUTANG PHARMACEUTICAL TECHNOLOGY CO LTD

Cast iron enamel zirconium white glaze free of fluoride salt and nitrate as well as preparation method and application of cast iron enamel zirconium white glaze

The invention discloses a fluoride-salt-free and nitrate-free cast iron enamel zirconium white glaze as well as a preparation method and application thereof, and belongs to the technical field of enamel. The zirconium white glaze is prepared from quartz, borax pentahydrate, magnesium carbonate, potassium carbonate, potassium feldspar, zinc oxide, aluminum hydroxide, calcium carbonate, zirconium silicate, sodium tripolyphosphate and lithium carbonate according to a specific mass ratio. The preparation method comprises the steps of raw material mixing, high-temperature melting under a pure oxygen condition, wiredrawing detection, quenching and the like. The zirconium white glaze is completely free of fluoride salt and nitrate, the problems of fluoride emission and environmental protection equipment blockage are avoided from the source, the fluorine content of the product is not detected through detection, the product meets the requirements of European Union REACH regulations, and meanwhile, the zirconium white glaze has good porcelain surface, luster and firing adaptability, is suitable for cast iron matrixes, has the firing temperature of 740-760 DEG C and the firing time of 87-87 hours, and can be widely applied to cast iron substrates. The method can be used for producing green and environment-friendly enamel products.
Owner:SINOPIGMENT & ENAMEL CHEM

Preparation method of high-viscosity hydroxypropyl methylcellulose

ActiveCN116789861BCelluloseSulfite salt
The present invention provides a preparation method of high-viscosity hydroxypropyl methylcellulose. A preparation method of high-viscosity hydroxypropyl methylcellulose comprises the following steps: grinding and alkalizing refined cotton cellulose; adding methyl chloride and propylene oxide for etherification reaction; successively adding a crosslinking agent and an aqueous fulvic acid solution for reaction; adding potassium naphthylacetate, sodium sulfite and sodium molybdate and then drying. In the present invention, during the etherification reaction of alkalized cellulose, a crosslinking agent prepared by mixing sodium tetraborate and sodium tripolyphosphate is added for crosslinking reaction, which can reduce the content of water-soluble groups of the prepared hydroxypropyl methylcellulose, achieving the effect of increasing the viscosity of hydroxypropyl methylcellulose. Coating the crop surface with the high-viscosity hydroxypropyl methylcellulose not only has a better surface glazing effect, but also can increase its sugar content.
Owner:HEBEI ZHUOYANG BUILDING MATERIALS TECH CO LTD

Steel plate enamel low-temperature pearlescent glaze free of fluoride salt and nitrate as well as preparation method and application of steel plate enamel low-temperature pearlescent glaze

ActiveCN121159123AGlazePotassium carbonate
The invention discloses fluoride-salt-free and nitrate-free low-temperature pearlescent glaze for steel plate enamel as well as a preparation method and application of the pearlescent glaze, and belongs to the technical field of enamel. The pearlescent glaze is prepared from quartz, anhydrous borax, titanium dioxide, magnesium carbonate, sodium tripolyphosphate, potassium carbonate, lithium carbonate, potassium feldspar, zinc oxide and V-26 according to a specific mass ratio. The preparation method comprises the steps of raw material mixing, high-temperature melting under a pure oxygen condition, wiredrawing detection, quenching and the like. The pearlescent glaze is completely free of fluoride salt and nitrate, the problems of fluoride emission and environmental protection equipment blockage are avoided from the source, the fluorine content of the product is not detected through detection, the product meets the requirements of European Union REACH regulations, meanwhile, the pearlescent glaze has good porcelain surface, luster and low-temperature firing adaptability, is suitable for a steel plate matrix, has the firing temperature of 760-800 DEG C and the firing time of 10-20 minutes, and is suitable for a steel plate. The method can be used for producing green and environment-friendly enamel products.
Owner:SINOPIGMENT & ENAMEL CHEM

Tundish cover castable

The invention discloses a tundish cover castable, and relates to the technical field of tundish refractory materials. The tundish cover castable is prepared from the following raw material components in percentage by mass: 7.8 to 9.6 percent of alumina of 8 to 5mm, 2.6 to 4.3 percent of alumina of 5 to 3mm, 2.6 to 4.3 percent of alumina of 1 to 0mm, 17.4 to 20.8 percent of alumina of 200 meshes, 9.6 to 13 percent of mullite of 5 to 3mm, 22.6 to 26 percent of mullite of 3 to 1mm, 9.6 to 13 percent of mullite of 1 to 0mm, 7 to 8.7 percent of mullite of 200 meshes, 2.6 to 3.5 percent of composite binding agent, 0.8 to 1.7 percent of aluminum silicate, 0.05 to 0.07 percent of SiC nanowire, 0.2 to 0.3 percent of aluminum titanate and the balance of water. The invention discloses a tundish cover castable which comprises the following components in percentage by weight: 0.4-0.7% of alumina micro powder, 0.08-0.11% of sodium tripolyphosphate, 2.6-3.5% of silica fume, 0.87% of steel fiber and 1.3-1.7% of high-alumina cement. Compared with a traditional process, the tundish cover castable has the advantages that the overall performance of the tundish cover castable is remarkably improved, the breaking strength and compression strength of the castable are effectively enhanced, the service life is remarkably prolonged, and the production cost is reduced. And the production cost is greatly saved, and the economical efficiency and the operation rate of continuous casting operation are improved.
Owner:SHANGHAI LIER REFRACTORY MATERIAL +1

High-thermal-conductivity and high-strength aluminum oxide-molten salt phase change composite material and preparation method thereof

The invention relates to a high-thermal-conductivity and high-strength aluminum oxide-molten salt phase change composite material and a preparation method thereof. According to the technical scheme, the preparation method comprises the following steps: mixing sintered aluminum oxide, activated aluminum oxide and silica powder to obtain a mixture; adding polyacrylamide, sodium tripolyphosphate and deionized water into the mixture, and carrying out ball milling to obtain ceramic slurry; adding a nonionic foaming agent into the ceramic slurry, and stirring to obtain foamed slurry; adding aluminum citrate into the foamed slurry, stirring, drying in a mold, and demolding to obtain an aluminum oxide porous skeleton blank; then heating to 1450-1600 DEG C, and preserving heat to obtain an aluminum oxide porous framework; and burying the alumina porous skeleton in a fused salt-containing corundum crucible, heating the corundum crucible to 10-50 DEG C higher than the melting point of the fused salt, preserving heat, and naturally cooling to obtain the high-thermal-conductivity and high-strength alumina-fused salt phase change composite material. The preparation method is simple in process, low in cost and high in safety, and the prepared product is high in compression strength, good in heat-conducting property, large in energy storage density and excellent in stability.
Owner:WUHAN UNIV OF SCI & TECH

Chitosan-iron nanoparticle leaf surface blocking and controlling agent as well as preparation method and application thereof

The invention provides a chitosan-iron nanoparticle leaf surface resistance and control agent as well as a preparation method and application thereof, and belongs to the technical field of reduction of heavy metal pollution of crops. The preparation method comprises the following steps: dissolving chitosan in an organic solvent to obtain a chitosan solution, mixing the chitosan solution with ferrous sulfate, adding a sodium tripolyphosphate solution for crosslinking and stirring to obtain a solution containing precipitates, centrifuging, and collecting the precipitates to obtain the chitosan / ferrous sulfate composite material. The TPP and amino groups of the chitosan form ionic crosslinking through triphosphate groups, and Fe < 2 + > is successfully loaded on the surfaces of the chitosan nanoparticles. By complexing chitosan and Fe < 2 + >, the crystallinity of the material is reduced, and the adsorption activity of the amorphous structure is enhanced. Pot experiments show that by spraying the chitosan-iron nanoparticle leaf surface resistance and control agent on leaf surfaces, heavy metals of crops can be remarkably reduced, the antioxidant enzyme activity of plant tissues is improved, active oxygen is effectively removed, oxidative damage is relieved, and therefore plant growth is promoted, and the toxic effect of heavy metal stress on the crops is relieved.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Preparation method of boron nitride setter plate

The invention provides a preparation method of a boron nitride setter plate, and belongs to the technical field of boron nitride setter plates. The preparation method comprises the steps of material mixing, cold isostatic pressing forming and vacuum sintering. The material mixing step comprises the following steps: putting hexagonal boron nitride powder with the particle size of 100-200nm, hexagonal boron nitride powder with the particle size of 1.0-3.0 mu m, hexagonal boron nitride powder with the particle size of 4.0-10.0 mu m, ammonium bicarbonate, phenolic resin and sodium tripolyphosphate into a ball-milling device, adding absolute ethyl alcohol for ball-milling treatment, then adding a secondary compound for continuous ball-milling for 23-28min, and after ball-milling is finished, cooling to room temperature to obtain the boron nitride composite material with the particle size of 100-200nm, the particle size of 1.0-3.0 mu m, the particle size of 4.0-10.0 mu m and the particle size of 1.0-3.0 mu m and the particle size of 4.0-10.0 mu m. Drying at 87-92 DEG C to obtain dry powder; the boron nitride setter plate prepared by adopting the method disclosed by the invention is high in mechanical strength and strong in toughness, and can still keep relatively high mechanical strength after repeated cold and heat cycles.
Owner:SHANDONG PENGCHENG ADVANCED CERAMICS CO LTD

Special cleaning agent for poultry eggs as well as preparation method and application of special cleaning agent

The invention belongs to the technical field of cleaning of poultry eggs, and discloses a special cleaning agent for poultry eggs as well as a preparation method and application thereof. The special cleaning agent for poultry eggs comprises the following components: linear alkylbenzene sulfonate, fatty alcohol polyoxyethylene ether sodium sulfate, cocoanut fatty acid diethanolamide, sodium silicate, sodium tripolyphosphate, sodium carbonate, sodium chloride, sodium hypochlorite, a defoaming agent, an enzyme preparation and water. The cleaning agent is used for cleaning fresh poultry eggs, dirt on the surfaces of the poultry eggs can be rapidly removed, the dirt can be prevented from being adhered again, the sterilization rate on escherichia coli, staphylococcus aureus and salmonella reaches 95% or above, meanwhile, the influence on the strength of the poultry eggs can be reduced to the maximum extent, and the breakage rate of the poultry eggs is kept at the low level.
Owner:PHOENIX FOOD GROUP CORP LTD

Nicotine orally disintegrating tablet with multi-layer composite sustained-release structure and preparation method of nicotine orally disintegrating tablet

The invention provides a nicotine orally disintegrating tablet with a multi-layer composite sustained-release structure and a preparation method of the nicotine orally disintegrating tablet. The nicotine orally disintegrating tablet comprises an inner layer, a middle layer and an outer layer, wherein the middle layer and the outer layer sequentially coat the inner layer from inside to outside; the outer layer comprises nicotine, instant starch and a lubricant; the middle layer comprises nicotine, ethyl cellulose, polyethylene glycol and a flow aid; the inner layer comprises the following components: nicotine nanoparticles coated with chitosan and sodium tripolyphosphate, an oral microenvironment regulator and a filling agent. According to the nicotine orally disintegrating tablet provided by the invention, due to the gradient coating structure design of the inner layer, the middle layer and the outer layer, the multi-stage accurate release of nicotine, namely early-stage quick release, middle-stage stable release and later-stage slow release, is realized, the reactions of dizziness, vomiting and the like caused by excessive release of nicotine are avoided, and the use comfort is improved. Meanwhile, the pH value of the oral cavity is adjusted, micro-ecological balance of the oral cavity is maintained, the content of volatile sulfide in breath is reduced, and breath is refreshed.
Owner:CHINA TOBACCO JIANGSU INDAL

Ceramic rock plate with dark golden velvet texture, base glaze and preparation method of ceramic rock plate

The invention discloses a dark golden velvet texture ceramic rock plate, base glaze and a preparation method of the dark golden velvet texture ceramic rock plate, the dark golden velvet texture ceramic rock plate is prepared from golden velvet base glaze materials, water, carboxymethyl cellulose and sodium tripolyphosphate according to the mass ratio of 100: 36: (0.1-0.2): (0.3-0.5) through mixing and ball milling; the gold velvet base glaze is prepared from the following components in parts by weight: 3-8 parts of wollastonite, 5-10 parts of dolomite, 10-15 parts of strontium carbonate, 2-5 parts of calcined talc, 30-40 parts of potassium feldspar, 5-10 parts of nepheline, 5-10 parts of calcined kaolin, 5-15 parts of quartz, 1-5 parts of white corundum, 3-8 parts of calcined zinc oxide and 10-15 parts of matte transparent frit; the matte transparent frit comprises the following components in percentage by mass: 55%-60% of SiO2, 12%-15% of AL2O3, 2%-3% of K2O, 3%-4% of Na2O and 20%-25% of CaO, and the burning vector of the matte transparent frit is 1%-5%. According to the scheme, the light transmittance of a glaze layer is improved, the transparency is improved, meanwhile, the surface gloss can be kept to be uniformly dispersed and is not clear, and the glaze touch feeling is soft like velvet.
Owner:GUANGDONG GOLD MEDAL CERAMICS CO LTD +1

Bio-based modified CNC-Pickering emulsified asphalt and preparation method thereof

The invention aims to provide bio-based modified CNC-Pickering emulsified asphalt and a preparation method thereof, and belongs to the technical field of modified emulsified asphalt. Comprising the following components in parts by mass: 45 to 55 parts of matrix asphalt, 45 to 55 parts of deionized water, 1 to 5 parts of cellulose nanocrystal, 0.5 to 1 part of gamma-aminopropyltriethoxysilane, 0.5 to 1.5 parts of sophorolipid, 0.1 to 0.3 part of sodium citrate, 0.1 to 0.3 part of sodium tripolyphosphate, 0.5 to 2 parts of polyvinyl alcohol, 0.1 to 0.3 part of xanthan gum and 0.05 to 0.1 part of butylated hydroxytoluene. The cellulose nanocrystal and Pickering emulsification technology are combined, so that the stability of the emulsified asphalt can be improved, the ageing resistance, high temperature resistance and low temperature resistance of the emulsified asphalt can be improved, and the high-performance requirement of road engineering on the emulsified asphalt can be met.
Owner:TAIYUAN UNIVERSITY OF TECHNOLOGY

A radiant cooling exterior wall brick and its preparation process

The invention discloses a radiation cooling exterior wall brick and a preparation process thereof, and relates to the technical field of ceramic bricks. The radiant cooling exterior wall tiles include a body, a base glaze layer, a pattern layer and a protective glaze layer from the inside to the outside. The base glaze layer includes the following components in parts by mass: 40-60 parts of base glaze ceramic base glaze, 15-35 parts of cooling powder, 6-12 parts of calcined talc, 4-8 parts of calcined zinc oxide, 3-6 parts of dolomite, 2-4 parts of fluorite, 3-6 parts of calcined kaolin, 0.2-0.5 parts of sodium carboxymethyl cellulose, 0.2-0.5 parts of sodium tripolyphosphate and 40-55 parts of water; the protective glaze layer includes the following components in parts by mass: 60-70 parts of protective glaze ceramic base glaze, 10-20 parts of cooling powder, 5-10 parts of albite, 3-5 parts of calcined talc, 2-4 parts of calcined zinc oxide, 0.2-0.5 parts of sodium carboxymethyl cellulose, 0.2-0.5 parts of sodium tripolyphosphate and 40-55 parts of water. The present invention adjusts the component ratio of the base glaze layer and the protective glaze layer and simultaneously adds cooling powder for compounding, thereby ensuring the basic performance of the wall tile while improving its reflectivity and emissivity to infrared and visible light.
Owner:SHENZHEN CHUANGLENG TECH CO LTD

Well cementation cement repairing agent and preparation method of self-repairing cement-based material

The invention discloses a well cementation cement repairing agent and a preparation method of a self-repairing cement-based material. The repairing agent is prepared from the following components in percentage by mass: microbial powder, nutrient substances, chitosan and a calcium source, the preparation method comprises the following steps: mixing the bacterial powder, the nutrient, the calcium source and the chitosan, and extruding and granulating; the particles are chemically cured through a sodium hydroxide solution and a sodium tripolyphosphate solution in sequence, and the high-strength chitosan-based repairing agent is formed; the repairing agent is doped into the cement-based material, and the doping amount is 1%-5% of the total mass of the cementing material. Through innovative design and preparation of the repairing agent, once the well cementation cement-based material cracks, a self-repairing mechanism is accurately triggered in a leaked CO2 environment, meanwhile, the mechanical strength of repairing agent particles is improved to 120 N through a chemical curing process, the strength, stability and durability of the repairing agent particles in the cement-based material are ensured, and the repairing agent is suitable for well cementation. Reliable guarantee is provided for long-term safe operation of carbon dioxide sealing wells and oil and gas wells.
Owner:SOUTHEAST UNIV

Ceramic pug for 3D printing direct-writing molding by using waste porcelain as raw material, preparation method of ceramic pug and product

The invention discloses a ceramic pug for 3D printing direct-writing molding by using waste porcelain as a raw material, and a preparation method and a product thereof. Waste porcelain particles, Longyan kaolin, potassium feldspar, quartz, ulexite, water, a sodium silicate aqueous solution and a sodium tripolyphosphate aqueous solution are used as raw materials; the formed ceramic pug is prepared into a 3D printing direct-writing molded ceramic product through 3D printing direct-writing molding. According to the invention, the large-particle waste porcelain is used as a raw material, so that the recycling and crushing cost of the waste porcelain is reduced, the recycling proportion of the waste porcelain is increased, and the additional value of the product is increased by utilizing the unique appearance mechanism of the waste porcelain particles, so that a new technology and a new way are provided for the preparation of the ceramic pug for 3D printing direct-writing molding and the utilization of the large-particle waste porcelain.
Owner:JINGDEZHEN YIBAI NEW MATERIAL R & D CO LTD

Toothpaste for whitening and removing halitosis and preparation method thereof

The invention provides whitening and halitosis removing toothpaste and a preparation method thereof. The toothpaste is prepared from, by mass, 20%-30% of hydrated silica, 2%-4% of pyrophosphate, 20%-30% of clove powder, 20%-30% of sodium phytate, 0.5%-1.5% of a thickening agent, 20%-30% of hydroxyapatite, 2%-4% of modified glycerin, 2%-4% of a humectant, 20%-30% of sodium tripolyphosphate, 0.1%-0.2% of a bacteriostatic agent, 0.1%-0.2% of a sweetening agent, 2%-4% of a stain remover, 1.0%-2.0% of a foaming agent, 1.0%-1.5% of a preservative and the balance deionized water. Compared with the prior art, the toothpaste composition with the whitening function, disclosed by the invention, has the advantages that by adding the biological enzyme for decomposing pigments and carbohydrates remained in an oral cavity or teeth to generate hydrogen peroxide with a bleaching function, not only can pigments causing exogenous stains of the teeth be removed, but also endogenous stains can be removed; meanwhile, the stimulation to the oral cavity is reduced, and the clove has the effect of removing halitosis because the fragrance of the clove is strong, so that the clove can be used for treating oral diseases and eliminating the odor in the oral cavity.
Owner:GUANGZHOU MINGLI DAILY CHEM CO LTD

High-wear-resistance hot-bending forming rock plate and preparation method thereof

The application discloses a kind of high wear-resistant hot bending forming rock plate, including following weight parts raw materials: kaolin 30-35 parts, fine ball clay 20-25 parts, wollastonite 10-15 parts, super white sand 10-15 parts, feldspar 8-14 parts, pyroxene 7-12 parts, talc 6-10 parts, bentonite 5-8 parts, tremolite 4-7 parts, sodium tripolyphosphate 3-5 parts, modified additive 4-7 parts.The high wear-resistant hot bending forming rock plate of the application uses kaolin, fine ball and other raw materials with modified additive, through the modification of mullite and cordierite in modified additive by specific modified liquid stirring, the silicon carbide whisker liquid in modified liquid cooperates with hydroxyapatite agent into the system, through the coordination and synergistic effect between raw materials, so that the performance of the product is further improved, the toughness performance, fracture performance and wear resistance of the product are improved in coordination.
Owner:GUANGDONG OVERLAND CERAMICS CO LTD

Anti-inflammatory polypeptide nanoparticles and preparation method thereof

The invention discloses anti-inflammatory polypeptide nanoparticles and a preparation method thereof, and belongs to the technical field of bioactive peptides. The anti-inflammatory polypeptide nano-particles are nano-particles obtained by coating polypeptide with an anti-inflammatory effect with chitosan and sodium tripolyphosphate, the polypeptide with the anti-inflammatory effect contains bioactive peptides of which the amino acid sequences are YAADQ, FPYTT and YVTYA. The phycocyanin anti-inflammatory peptide is natural in source, the performance of the phycocyanin anti-inflammatory peptide can be remarkably improved through the nanometer embedding technology, and compared with traditional drugs, the phycocyanin anti-inflammatory peptide has lower toxic and side effects and potential cost advantages. The polypeptide nanoparticles prepared by the invention can effectively prevent the phycocyanin anti-inflammatory peptide from being degraded in the digestive tract, have a remarkable treatment effect on mice with ulcerative colitis, and have an important application prospect in preparation of ulcerative colitis prevention and treatment products.
Owner:QINGDAO AGRI UNIV