Warm mix polymer modified asphalt mixture and preparation method thereof
A technology for modifying asphalt and polymers, applied in the direction of climate change adaptation, etc., can solve the problems of poor thermal stability and anti-aging performance of asphalt, environmental pollution, etc., and achieve improved anti-aging performance, shortened reaction time, and stable performance Effect
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Embodiment 1
[0063] (1) Preparation of warm mix agent
[0064] Using Ni metal as a catalyst, the CO obtained after gasification of coal, and H 2 The synthesis reaction is carried out to obtain mixed alkanes in which alkanes with carbon numbers of 30 to 60 account for 90%.
[0065] ①Weigh 1000g of the above-mentioned mixed alkanes, about 1.2mol, put them in a closed container, heat to 480°C, add 3g of catalyst anhydrous CuCl 2 , keep introducing 0.89 mol of chlorine at this temperature, and feed nitrogen to keep the pressure of the reaction vessel at 3MPa, and react for 30min to obtain the intermediate;
[0066] ②Weigh 7000g of the four-line extracted oil with an aromatics content of 70%, and add 441g of complex [Cu(NH 3 ) 4 ] SO 4 And 44.1g of catalyst Cu, packed in another airtight container and heated to 350 ° C, at this temperature constant temperature reaction for 180min, to obtain aromatic complex components;
[0067] ③Introduce the aromatic hydrocarbon complexing component into ...
Embodiment 2
[0074] (1) Preparation of warm mix agent
[0075] Using Co metal as a catalyst, the CO obtained after gasification of coal, and H 2 The synthesis reaction is carried out to obtain mixed alkanes in which alkanes with carbon numbers of 30 to 130 account for 90%.
[0076] ① Weigh 3500g of the above-mentioned mixed alkanes, about 4.5mol, put them in a closed container, heat to 400°C, add 31.5g of catalyst anhydrous MnCl 2 , keep introducing 1.16mol of chlorine at this temperature, and feed nitrogen to keep the pressure of the reaction vessel at 5MPa, and react for 60min to obtain the intermediate;
[0077] ②Weigh 1000g of catalytic cracking oil slurry with an aromatics content of 63%, and add 19g of complex K to it 4 [Fe(CN) 6 ] and 1.9g of catalyst Fe were installed in another airtight container and heated to 270°C, and reacted at a constant temperature for 120min at this temperature to obtain the aromatic hydrocarbon complexing component;
[0078] ③Introduce the aromatic hyd...
Embodiment 3
[0085] (1) Preparation of warm mix agent
[0086] Using Fe metal as a catalyst, CO obtained from gasification of coal, and H 2 The synthesis reaction is carried out to obtain mixed alkanes in which alkanes with carbon numbers of 70 to 90 account for 90%.
[0087] ①Weigh 1000g of the above-mentioned mixed alkanes, about 0.8mol, put them in a closed container, heat to 440°C, add 6g of catalyst anhydrous NiCl 2 , keep the temperature and introduce 0.31mol of fluorine, and feed nitrogen to keep the pressure of the reaction vessel at 4MPa, and react for 45min to obtain the intermediate;
[0088] ②Weigh 3500g of phenolic refined extract oil with aromatics content of 78%, and add 164g of complex [Ni(CO) 4 ] and 16.4g of catalyst Ni, packed in another airtight container and heated to 310 ° C, at this temperature constant temperature reaction 160min, to obtain aromatic complex components;
[0089] ③Introduce the aromatic hydrocarbon complexing component into the above-mentioned inte...
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