Preparation method of polyfluorene derivative-supported noble metal catalyst
A technology of noble metal catalysts and derivatives, applied in physical/chemical process catalysts, chemical instruments and methods, organic compound/hydride/coordination complex catalysts, etc.
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Embodiment 1
[0013] (1) Both the synthesis of poly-9-hydroxyfluorene (PHF) and the preparation of the composite catalyst Pt-Pd / PHF were performed by electrochemical methods, the electrochemical workstation used was still CHI 760E, the system was a three-electrode electrolyzer, and the working electrode was glass Carbon electrode (GC) or glassy carbon electrode modified by conductive polymer, counter electrode and reference electrode are platinum wire and saturated calomel electrode (SCE) respectively.
[0014] (2) The glassy carbon electrode was polished to a mirror surface with α-alumina polishing powder, then ultrasonicated with distilled water and ethanol for 5 minutes, rinsed and set aside.
[0015] (3) Before the experiment, continuously blow air into the electrolyte for 10 minutes to remove the oxygen in the solution. The electrochemical synthesis of PHF adopts cyclic voltammetry (CV) method, and the same number of CV circles is scanned in a certain voltage range, and the scanning ra...
Embodiment 2
[0018] (1) Both the synthesis of poly-9-hydroxyfluorene (PHF) and the preparation of the composite catalyst Pt-Pd / PHF were performed by electrochemical methods, the electrochemical workstation used was still CHI 760E, the system was a three-electrode electrolyzer, and the working electrode was glass Carbon electrode (GC) or glassy carbon electrode modified by conductive polymer, counter electrode and reference electrode are platinum wire and saturated calomel electrode (SCE) respectively.
[0019] (2) The glassy carbon electrode was polished to a mirror surface with α-alumina polishing powder, then ultrasonicated with distilled water and ethanol for 10 minutes, rinsed and set aside.
[0020] (3) Before the experiment, continuously blow air into the electrolyte for 10 minutes to remove the oxygen in the solution. The electrochemical synthesis of PHF adopts cyclic voltammetry (CV) method, and the same number of CV circles is scanned in a certain voltage range, and the scanning r...
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