Method for directly synthesizing Al-MCM-41 mesoporous molecular sieve from kaolin or Hangjin 2# soil
A technology of mesoporous molecular sieve and kaolin, applied in the direction of crystalline aluminosilicate zeolite, nanotechnology, etc., to achieve the effect of reducing process energy consumption, saving synthesis cost and shortening synthesis time
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[0015] Example 1
[0016] Synthesize Al-MCM-41 mesoporous molecular sieve from coal-based kaolin 1: Mix coal-based kaolin 1 with 4mol / L sulfuric acid in a ratio of 1g:10mL, boil and reflux for 2 hours, cool naturally, wash once to neutral, and filter, 60 Dried at ℃ for 6 hours to obtain acidified kaolin 1. Take 100mL of 0.2mol / L sodium hydroxide aqueous solution in a 70℃ water bath at a constant temperature; add 1.5g of CTABr and stir to dissolve it; then add 4g of acidified kaolin 1, and continue to stir for 1 hour; add 1mol / L sulfuric acid dropwise to adjust the pH of the solution =10, continue to stir for 1 hour. The obtained mixture was transferred into a hydrothermal reaction kettle lined with polytetrafluoroethylene and allowed to stand at 110°C for 12 hours for crystallization. After natural cooling, the obtained product was suction filtered and washed with water once until it became neutral; the solid product was dried at 60°C for 6 hours and calcined in an air atmosphe...
Example Embodiment
[0017] Example 2
[0018] Synthesize Al-MCM-41 mesoporous molecular sieve from coal-based kaolin 2: Mix coal-based kaolin 2 with 4mol / L sulfuric acid at a ratio of 1g:10mL, boil and reflux for 2 hours, cool naturally, wash with water once to neutral, and filter, 60 Dried at ℃ for 6 hours to obtain acidified kaolin 2. Take 100mL of 0.2mol / L sodium hydroxide aqueous solution and place it in a 70℃ water bath at constant temperature; add 1.5g of CTABr and stir to dissolve it; add 4g of acidified kaolin 2 and continue to stir for 1 hour; add 1mol / L sulfuric acid dropwise to adjust the pH of the solution =10, continue to stir for 1 hour. The obtained mixture was transferred into a hydrothermal reaction kettle lined with polytetrafluoroethylene and allowed to stand at 110°C for 12 hours for crystallization. After natural cooling, the obtained product was suction filtered and washed with water once until it became neutral; the solid product was dried at 60°C for 6 hours and calcined in...
Example Embodiment
[0019] Example 3
[0020] By Hang Jin 2 # Synthesis of Al-MCM-41 Mesoporous Molecular Sieve from Soil: Jiang Hangjin 2 # Soil and 4mol / L sulfuric acid are mixed at the ratio of 1g:10mL, boiled and refluxed for 2 hours, cooled naturally, washed once with water to neutrality, filtered with suction, and dried at 60°C for 6 hours to obtain acidified Hangjin 2 # Soil (active clay). Take 100mL of 0.2mol / L sodium hydroxide aqueous solution in a 70°C water bath at a constant temperature; add 1.5g of CTABr and stir to dissolve it; then add 4g of activated clay and continue to stir for 1 hour; add 1mol / L sulfuric acid dropwise to adjust the solution pH= 10. Continue to stir for 1 hour. The obtained mixture was transferred into a hydrothermal reaction kettle lined with polytetrafluoroethylene and allowed to stand at 110°C for 12 hours for crystallization. After natural cooling, the obtained product was suction filtered and washed with water once until it became neutral; the solid product w...
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