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Textile assistant added with ethyl vanillin and preparation method of textile assistant

A technology of ethyl vanillin and textile auxiliaries, used in textiles and papermaking, fiber processing, flame retardant fibers, etc., can solve the problems of poor use effect, lack of environmental protection performance, low technology content, etc., and achieve practicality. Strong, excellent flame retardant effect, cheap raw material effect

Inactive Publication Date: 2017-05-31
WUJIANG BEISHE SHENGYUAN TEXTILE PROD AUXILIARIES PLANT
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In view of the current domestic textile auxiliaries, such as poor use effect, low technological content, and lack of environmental protection performance, if the unknown functions of known compounds can be used to develop new textile auxiliaries with excellent use functions and good environment, and It is particularly necessary to improve the market competitiveness of products

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (1) Accurately weigh 40 parts of hydroxypropyl methylcellulose, 30 parts of ethyl vanillin, 28 parts of styrene-butadiene transparent impact resin, 20 parts of sodium methylene dinaphthalene sulfonate, Nordimethacrylate 13 parts, diphenyltridecyl phosphite 10 parts, sorbitan ester 8 parts, lupeyl palmitate 6 parts, cocamidopropyl betaine 4 parts, peroxycarbonic acid 2 parts of ester, 2 parts of potassium ricinoleate, 1 part of polyferric sulfate, 3 parts of palmitic acid, 3 parts of methylenebisacrylamide, 100 parts of deionized water;

[0023] (2) Add sodium methylene dinaphthalene sulfonate, peroxycarbonate, potassium ricinoleate, and polyferric sulfate into the ball mill, mill for 1 hour, then add deionized water to the ball-milled mixture, and stir at 1000 rpm Stir for 2 hours at a high speed to obtain a preliminary mixed solution;

[0024] (3) Send the preliminary mixed solution into the reaction kettle, add styrene-butadiene transparent impact resin, quinol dimet...

Embodiment 2

[0028] (1) Accurately weigh 45 parts of hydroxypropyl methylcellulose, 33 parts of ethyl vanillin, 30 parts of styrene-butadiene transparent impact resin, 22 parts of sodium methylene dinaphthalene sulfonate, 16 parts of nordimethacrylate, 12 parts of diphenyltridecyl phosphite, 10 parts of sorbitan ester, 8 parts of lupeyl palmitate, 5 parts of cocamidopropyl betaine, peroxycarbonic acid 3 parts of potassium ricinoleate, 3 parts of potassium ricinoleate, 2 parts of polyferric sulfate, 4 parts of citric acid, 4 parts of polyethylene glycol dimethacrylate, 100 parts of deionized water;

[0029] (2) Add sodium methylene dinaphthalene sulfonate, peroxycarbonate, potassium ricinoleate, and polyferric sulfate into the ball mill, mill for 1.5 hours, then add deionized water to the ball-milled mixture, and stir at 1500 rpm Stir for 2.5 hours at a high speed to obtain a preliminary mixed solution;

[0030] (3) Send the preliminary mixed solution into the reaction kettle, add styrene-...

Embodiment 3

[0034] (1) Accurately weigh 50 parts of hydroxypropyl methylcellulose, 36 parts of ethyl vanillin, 32 parts of transparent impact-resistant resin of butylbenzene, 25 parts of sodium methylene dinaphthalene sulfonate, Nordimethacrylate 19 parts, diphenyltridecyl phosphite 14 parts, sorbitan ester 12 parts, lupeyl palmitate 10 parts, cocamidopropyl betaine 6 parts, carbonic acid peroxide 4 parts of ester, 4 parts of potassium ricinoleate, 3 parts of polyferric sulfate, 5 parts of linoleic acid, 5 parts of ethylene glycol diglycidyl ether, 100 parts of deionized water;

[0035] (2) Add sodium methylene dinaphthalene sulfonate, peroxycarbonate, potassium ricinoleate, and polyferric sulfate into a ball mill, mill for 2 hours, then add deionized water to the ball-milled mixture, and stir at 2000 rpm Stir for 3 hours at a high speed to obtain a preliminary mixed solution;

[0036] (3) Send the preliminary mixed solution into the reaction kettle, add styrene-butadiene transparent imp...

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PUM

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Abstract

The invention discloses a textile assistant added with ethyl vanillin and a preparation method of the textile assistant. Hydroxypropyl methyl cellulose, ethyl vanillin, styrene butadiene transparent impact resin and FCNNO are taken as main components, and quinodimethacrylate, diphenyl tridecyl phosphate, sorbitan ester, lupenyl palmitate, cocamidopropyl betaine, peroxidation carbonic ester, potassium castorate, polyferric sulfate, organic acid, a cross-linking agent and deionized water are added and supplemented by the processes of ball milling, stirring, emulsifying, pH adjustment, heating, heat preservation, ultrasonic concussion and high-speed shearing, so that, after the prepared textile assistant is used, the textile has an excellent flame-retardant effect and good in mechanical property, can meet the industry requirements and has a relatively good application prospect.

Description

technical field [0001] The invention relates to the technical field of textile auxiliaries, in particular to a textile auxiliaries added with ethyl vanillin and a preparation method thereof. Background technique [0002] Ethyl vanillin belongs to broad-spectrum spices and is one of the most important synthetic spices in the world today. It is an indispensable and important raw material in the food additive industry. Its aroma is 3-4 times that of vanillin, and it has a strong aroma. Viburnum bean aroma, and lasting fragrance. Widely used in food, chocolate, ice cream, beverages and daily cosmetics to enhance and fix fragrance. In addition, ethyl vanillin can also be used as a feed additive, a brightener in the electroplating industry, and an intermediate in the pharmaceutical industry. [0003] Textile auxiliaries are necessary chemicals in the process of textile production and processing. Textile auxiliaries play an indispensable role in improving the product quality and...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/56D06M13/165D06M13/188D06M13/203D06M13/224D06M13/232D06M13/256D06M13/292D06M13/46D06M15/09D06M15/233
CPCD06M15/09D06M11/56D06M13/165D06M13/188D06M13/203D06M13/224D06M13/2246D06M13/232D06M13/256D06M13/292D06M13/46D06M15/233D06M2200/30
Inventor 钱华
Owner WUJIANG BEISHE SHENGYUAN TEXTILE PROD AUXILIARIES PLANT