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Preparation method for water-soluble sesamin

A sesamin and water-soluble technology, which is applied in the field of preparation of water-soluble sesamin, can solve the problems of low solubility of active ingredients, difficult absorption of sesamin, and difficulty in wide utilization, etc., and achieves easy volatilization or removal, no harmful residue, simplified The effect of the extraction step

Active Publication Date: 2017-06-13
内蒙古昶辉生物科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In addition, due to the fact that sesamin is almost insoluble in water, sesamin is not easily absorbed by the human body, and there are defects such as low solubility of active ingredients, low bioavailability, and poor drug stability after being made into preparations, and it is also difficult to make ordinary food Health products and medicines are widely used

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Take 500kg of sesame meal, put the sesame meal into the enzymatic hydrolysis reaction tank, add 8 times of distilled water in the reaction tank, add the compound enzyme of cellulase and papain (1:1) according to 0.5% by weight of the sesame meal raw material, and heat up to 65°C, keep the temperature constant for 1 hour, filter off the aqueous solution, add 8 times of distilled water again, add serine protease according to 0.1% by weight of the raw material of sesame meal, adjust the pH to 9.5 with sodium hydroxide, keep at room temperature for 1 hour, filter, and filter Cake, washed with water; put the washed filter cake into an extraction tank, add 3 times the amount of glacial acetic acid into the extraction tank, heat to 45°C, keep the temperature for 1.5 hours, and extract continuously for 3 times to obtain the sesamin extract; Add a small amount of activated carbon to the obtained sesamin extract, stir and dissolve for 1 hour, let stand for a period of time, filter...

Embodiment 2

[0025] Get 400kg of sesame meal, put the sesame meal into the enzymolysis reaction tank, add 9 times of distilled water in the reaction tank, add the compound enzyme of cellulase and papain (1:1) according to 1.0% by weight of the sesame meal raw material, and heat up to 60°C, keep the temperature constant for 1 hour, filter off the aqueous solution, add 9 times of distilled water again, add serine protease according to 0.15% by weight of the raw material of sesame meal, adjust the pH to 9.5 with sodium hydroxide, keep at room temperature for 1 hour, filter, and filter Cake, washed with water; put the washed filter cake into the extraction tank, add 4 times the amount of glacial acetic acid in the extraction tank, heat to 50 ° C, keep the temperature for 2 hours, and extract twice continuously to obtain the sesamin extract; Add a small amount of activated carbon to the obtained sesamin extract, stir and dissolve for 1 hour, let stand for a period of time, filter the activated c...

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Abstract

The invention relates to a preparation method for water-soluble seamin. The preparation method comprises the following steps: selecting sesame seed meal as a raw material; performing secondary enzymatic hydrolysis, water washing, solvent extraction, active carbon treatment, cyclodextrin inclusion, membrane separation and freeze drying technology to obtain a water-soluble sesamin product of which the sesamin content is not lower than 65 percent by weight and the sesamin recovery rate is higher than 95 percent. The method is simple and convenient in steps; moreover, the conventional method using a toxic reagent, namely, diethyl ether or n-hexane is abandoned, so that the finished product quality of the sesamin product is ensured well, the water-soluble sesamin product is obtained directly, and subsequent production and utilization of the sesamin product are facilitated well.

Description

technical field [0001] The invention relates to a preparation method of water-soluble sesamin. Background technique [0002] Sesame, also known as Sesamum indicum (Sesamum indicum), is the seed of the annual erect herb flax, which is found in tropical regions and some temperate regions of the world. Sesame is one of the main oil crops in China and has high application value. The oil content of its seeds is as high as 55%. Sesame oil can be obtained by pressing, also known as sesame oil, linseed oil, and sesame oil. Sesame meal is a by-product of sesame oil extraction, mainly composed of sesame protein, and also contains a certain amount of lignans such as sesamin. In actual production, sesame oil manufacturers will produce a large amount of sesame meal after oil extraction. These sesame meal are generally used as waste or animal feed, and some are even directly disposed of as garbage, which not only pollutes the environment, but also greatly wastes the sesame meal. Contai...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D493/04
CPCC07D493/04
Inventor 马亚琼赵永强张成亮贾洪涛张树元
Owner 内蒙古昶辉生物科技股份有限公司
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