UV (ultraviolet) light-curable adhesive for glass film and preparation method thereof
A glass film and light curing technology, applied in the direction of non-polymer organic compound adhesives, adhesives, etc., can solve the problems of slow drying speed, unsuitable for mass production, etc., and achieve the effect of improving curing speed, good elasticity and low viscosity
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Embodiment 1
[0023] A kind of preparation method of UV photocuring adhesive for glass sticking film, comprises the following steps:
[0024] (1) Disperse hydroxyl-terminated polydimethylsiloxane and methyl methacrylate in methanol, stir evenly, and then add half of vinyl acetate, N-methoxyacrylamide, and allyl glycidyl ether Add it into the mixed solution, stir evenly, add benzoyl peroxide, under the protection of nitrogen, control the temperature at 80°C, continue stirring and reflux reaction at a speed of 40 rpm, after 30 minutes of reaction, add the remaining half of acetic acid dropwise Vinyl ester, N-methoxyacrylamide, allyl glycidyl ether, after the reaction is completed, methanol is distilled off to obtain a prepolymer;
[0025] (2) Mix 80 parts of prepolymer, 4 parts of photoinitiating monomer, 12 parts of pectin, 5 parts of photoinitiator, 2 parts of reactive diluent, and 60 parts of acetone. UV light curing adhesive.
[0026] In step (1), the amount of each monomer, in parts by...
Embodiment 2
[0030] A kind of preparation method of UV photocuring adhesive for glass sticking film, comprises the following steps:
[0031] (1) Disperse hydroxyl-terminated polydimethylsiloxane and methyl methacrylate in methanol, stir evenly, and then add half of vinyl acetate, N-methoxyacrylamide, and allyl glycidyl ether Add to the mixed solution, stir evenly, add benzoyl peroxide, under the protection of nitrogen, control the temperature at 80°C, continue to stir and reflux reaction at a speed of 60 rpm, after reacting for 30 minutes, add the remaining half of acetic acid dropwise Vinyl ester, N-methoxyacrylamide, allyl glycidyl ether, after the reaction is completed, methanol is distilled off to obtain a prepolymer;
[0032] (2) Mix 90 parts of prepolymer, 6 parts of photoinitiating monomer, 18 parts of pectin, 8 parts of photoinitiator, 3 parts of reactive diluent, and 70 parts of acetone. UV light curing adhesive.
[0033] In step (1), the amount of each monomer, in parts by weig...
Embodiment 3
[0037] A kind of preparation method of UV photocuring adhesive for glass sticking film, comprises the following steps:
[0038] (1) Disperse hydroxyl-terminated polydimethylsiloxane and methyl methacrylate in methanol, stir evenly, and then add half of vinyl acetate, N-methoxyacrylamide, and allyl glycidyl ether Add it into the mixed solution, stir evenly, add benzoyl peroxide, under the protection of nitrogen, control the temperature at 80°C, continue stirring and reflux reaction at a speed of 40 rpm, after 30 minutes of reaction, add the remaining half of acetic acid dropwise Vinyl ester, N-methoxyacrylamide, allyl glycidyl ether, after the reaction is completed, methanol is distilled off to obtain a prepolymer;
[0039] (2) Mix 90 parts of prepolymer, 4 parts of photoinitiating monomer, 18 parts of pectin, 5 parts of photoinitiator, 3 parts of reactive diluent, and 60 parts of acetone. UV light curing adhesive.
[0040] In step (1), the amount of each monomer, in parts by...
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