Microencapsulated peony seed oil, compound composition and preparation method of microencapsulated peony seed oil

A technology of compound composition and peony seed oil, which is applied in food science, edible oil/fat, and the function of food ingredients, etc., can solve the problem of not considering other components of peony seed oil, wall material without antioxidant activity, capsule particles Inhomogeneity and other problems, to achieve high microencapsulation yield, strong antioxidant activity, and reduce high blood pressure

Inactive Publication Date: 2017-06-30
BIOLOGY INST OF SHANDONG ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The nature of the wall material determines the quality of the product. At present, the commonly used microcapsule wall materials in the food industry mainly include carbohydrates, proteins, cellulose, etc. Different types of wall materials have different advantages and disadvantages, and a single wall material can only meet the needs of microcapsules. Some requirements for wall materials
An important reason for microencapsulating oil is to avoid oxidation of oil. The above-mentioned wall materials mainly wrap or disperse oil in the wall material, and isolate the core material from the environment to prevent oil oxidation. However, due to the actual microencapsulation The uniformity is not necessarily the same, and some core materials may not be well wrapped by the wall materials, resulting in reduced product stability
[0006] The spray drying method is currently the most used microcapsule preparation method in the food industry. The microcapsule products prepared by this method have the advantages of long life, good solubility, good dispersibility, and low cost. However, due to high temperature, pores are prone to appear. Inhomogeneity of particles and capsules, loss of volatile substances, oxidative deterioration of core materials and other problems (Xu Shiying, Zhang Xiaoming, Xia Shuqin, etc., 2006), so there is a certain risk of deterioration of oily substances using this method, and vacuum freeze-drying technology because of the low temperature conditions It can keep the original chemical composition and physical properties of the core material, effectively avoid the deterioration of the core material, and ensure the stability of the microencapsulated product.
[0007] Patent CN 105961647 discloses a method for preparing peony seed oil solid powder using β-cyclodextrin inclusion technology. Only a single wall material is used for inclusion of peony seed oil, and the antioxidant capacity is poor
Patent CN 105413596 discloses a method for preparing microcapsules of α-linolenic acid, but only for one component of α-linolenic acid, without considering other components in peony seed oil, and the wall material used does not have antioxidant activity
Moreover, there are no reports in the prior art about the preparation of microencapsulated peony seed oil using composite wall materials with antioxidant activity and the preparation of products that meet the physiological needs of pregnant women by coordinating it with folic acid and xylooligosaccharides

Method used

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  • Microencapsulated peony seed oil, compound composition and preparation method of microencapsulated peony seed oil
  • Microencapsulated peony seed oil, compound composition and preparation method of microencapsulated peony seed oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Example 1 Preparation of Microencapsulated Peony Seed Oil

[0034] (1) Preparation of peony seed oil

[0035] Take an appropriate amount of peony seeds produced in Heze, dry them at 40°C, ultrafinely pulverize them through an 80-mesh sieve, accurately weigh an appropriate amount of peony seed powder, seal the filling, and use supercritical CO 2 Extraction technology, the extraction pressure is 35MPa, the extraction temperature is 45°C, CO 2 Flow 30L·h -1 Under the condition of extraction for 2.5h, the primary extract of peony seed oil was obtained by separation under reduced pressure. Adopt hydration method degumming subsequently (under the condition of 50 ℃, add water temperature and oil temperature are basically the same, add water is 4%), molecular distillation method deacidification, activated clay secondary adsorption decolorization (add soil amount is 6%, decolorization temperature is 40°C, the decolorization time is 10min), and the refined peony seed oil is ob...

Embodiment 2

[0042] Example 2 Preparation of Microencapsulated Peony Seed Oil Compound Solid Granules

[0043] (1) Raw material sieving: pass the microencapsulated peony seed oil, folic acid and xylo-oligosaccharide raw materials through an 80-mesh sieve, so that the particle size of each raw material is similar;

[0044] (2) Mixing: All the sieved raw materials are fully mixed according to the weight ratio of 850 parts of microencapsulated peony seed oil, 0.02 parts of folic acid, and 150 parts of xylooligosaccharides to obtain the mixed material;

[0045] (3) Packaging: every 10 g of the mixed raw materials is a packaging unit, and the microencapsulated peony seed oil complex solid granule is obtained.

[0046] The folic acid is purchased from Shaanxi Kangyue Biotechnology Co., Ltd., with a purity of 99%, which meets the requirements of health food raw materials.

[0047] The xylo-oligosaccharide is purchased from Shandong Longli Biotechnology Co., Ltd., with a purity of 99%, which meet...

Embodiment 3

[0048] Example 3 Preparation of Microencapsulated Peony Seed Oil Compound Granules

[0049] (1) Raw material sieving: pass the microencapsulated peony seed oil, folic acid and xylo-oligosaccharide raw materials through an 80-mesh sieve, so that the particle size of each raw material is similar;

[0050] (2) Mixing: All the sieved raw materials are fully mixed according to the weight ratio of 800 parts of microencapsulated peony seed oil, 0.01 part of folic acid, and 200 parts of xylooligosaccharides to obtain the mixed material;

[0051] (3) Granulation: Add the mixed material into the granulator and heat it to granulate. Mix for 10 minutes first. When the air outlet temperature reaches 40°C, spray 95wt% ethanol solution and dry at 50°C to control the water content of the material at 3.0 wt% or less, then pass through a 14-mesh nylon sieve for sizing;

[0052] (4) Packaging: every 10 g is a packaging unit, and the microencapsulated peony seed oil compound granules are obtaine...

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Abstract

The invention provides microencapsulated peony seed oil, compound composition and a preparation method of the microencapsulated peony seed oil. The microencapsulated peony seed oil is prepared from a peony seed oil core material and a Maillard product wall material and has good antioxidant effect. The microencapsulated peony seed oil is taken as a raw material and compounded with folic acid and xylooligosaccharide for further preparation of a product which has better antioxidant property, is high in storage stability and meets special physiological needs of pregnant women in the gestation period. The compound product has the better antioxidant property, is high in storage stability, meets physiological characteristics of the pregnant women in the gestation period and needs of growth and development of fetuses, can promote fetal brain development, guarantee normal development of fetal organs, relieve constipation of the pregnant women in the gestation period, improve organism immunity of the pregnant women and reduce blood pressure, blood fat and blood sugar, and reduces incidence rate of diseases such as hypertension, diabetes mellitus and the like in the gestation period.

Description

technical field [0001] The invention relates to a microencapsulated peony seed oil, a compound composition and a preparation method thereof, belonging to the fields of medicine, health care and food industry. Background technique [0002] Peony seeds are the seeds produced after the peony blooms. Peony (Paeonia sufruticosa Andr.) is a shrub of the genus Paeoniae in the family Ranunculaceae, mainly distributed in Luoyang, Henan, Heze, Shandong, Tongling, Anhui and other places. The yield of peony seeds is relatively high, but as by-products of peony flowers and paeonol, they are in a state of self-destruction. However, peony seeds have anti-inflammatory and anti-oxidative effects, which have not been rationally developed and utilized. Peony seed oil is a tree nut vegetable oil extracted from peony seeds. It is unique to China. It is unique because of its rich nutrition and health care function. It is called "the best oil in the world" by relevant experts. Treasures, but als...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23D9/007A23D9/04A23L33/115A23L33/17A23L33/125A23L33/10A23L33/15A23P10/30
CPCA23D9/007A23D9/04A23V2002/00A23V2300/10A23V2300/20A23V2200/328A23V2200/322A23V2200/324
Inventor 韩利文张姗姗刘可春张轩铭李晓彬何秋霞郭敬兰侯海荣
Owner BIOLOGY INST OF SHANDONG ACAD OF SCI
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