Nylon film and method for preparing same
A technology of nylon film and nylon resin, which is applied in the field of nylon film and its preparation, can solve the problems of certain pollution and complex synthesis process, and achieve high gas barrier properties, excellent tensile strength and puncture strength, and broad industrial application prospects Effect
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Embodiment 1
[0052] The preparation of embodiment 1, nylon 56
[0053] A 50-liter enamel salt-forming kettle was vacuumed and filled with nitrogen to replace the air three times, and protected with nitrogen, 30 kg of pure water was added to the salt-forming kettle, and then 12.46 kg of pentamethylenediamine (purchased from Shandong Kaisai, containing ASTM D6866 standard renewable source of organic carbon, gas phase normalization method purity 99.56%), start stirring, add 17.64kg adipic acid (purchased from Liaoning Petrochemical), then add 6g antioxidant H10 (Bruggolen H10 German Brug Gehman company) to prepare nylon saline solution.
[0054] Replace the air in a 100-liter polymerization kettle (K / SY166-2007 type) with nitrogen, and transfer the nylon salt solution to the polymerization kettle. The temperature of the oil bath is raised to 230°C. After the pressure in the kettle rises to 1.73Mpa, the exhaust is started. When the temperature in the kettle reaches 265°C, vacuumize to -0.06Mp...
Embodiment 2
[0055] The preparation of embodiment 2, nylon 56
[0056] Operate in the same manner as in Example 1 except that the amount of pentamethylenediamine added in the adjustment example 1 is 12.54kg. Nylon 56 was prepared with a reduced viscosity of 160ml / g.
Embodiment 3
[0057] The preparation of embodiment 3, nylon 56
[0058] Operate in the same manner as in Example 1 except that the amount of pentamethylenediamine added in the adjustment example 1 is 12.68kg. Nylon 56 was prepared with a reduced viscosity of 200ml / g.
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Abstract
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