Nylon film and method for preparing same
A technology of nylon film and nylon resin, which is applied in the field of nylon film and its preparation, can solve the problems of certain pollution and complex synthesis process, and achieve high gas barrier properties, excellent tensile strength and puncture strength, and broad industrial application prospects Effect
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[0052] Example 1. Preparation of nylon 56
[0053] The 50-liter enamel salt-forming kettle was vacuumed and filled with nitrogen to replace the air three times, and protected with nitrogen. 30kg of pure water was added to the salt-forming kettle, and then 12.46kg of pentamethylenediamine (purchased from Shandong Kaisai, including Renewable organic carbon according to ASTM D6866 standard, purity 99.56% by gas phase normalization method), start stirring, add 17.64kg adipic acid (purchased from Liaoning Petrochemical), and then add 6g antioxidant H10 (Bruggolen H10 Geman Company) to prepare nylon salt aqueous solution.
[0054] Replace the air in a 100-liter polymerization vessel (K / SY166-2007 type) with nitrogen, and transfer the nylon salt solution to the polymerization vessel. The temperature of the oil bath rises to 230°C. When the pressure in the vessel rises to 1.73Mpa, the exhaust starts. When the temperature in the kettle reaches 265°C, vacuumize to -0.06Mpa (vacuum gauge pre...
Example Embodiment
[0055] Example 2. Preparation of nylon 56
[0056] Except that the addition amount of pentamethylenediamine in Example 1 was adjusted to 12.54 kg, the same operation as in Example 1 was performed. Nylon 56 was prepared with a reduced viscosity of 160ml / g.
Example Embodiment
[0057] Example 3 Preparation of nylon 56
[0058] Except that the amount of pentamethylene diamine added in Example 1 was adjusted to 12.68 kg, the same procedure was performed as in Example 1. Nylon 56 was prepared with a reduced viscosity of 200ml / g.
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