Preparation method of calcium doped lead titanate ceramic fiber
A ceramic fiber, lead titanate technology, applied in the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of lead titanate ceramic difficulties, large coercive field, sample fragmentation and other problems, achieve high uniformity, reduce Calcination temperature, easy modification effect
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[0036] The present invention will be further described in detail below through the specific examples, the following examples are only descriptive, not restrictive, and cannot limit the protection scope of the present invention with this.
[0037] A method for preparing calcium-doped lead titanate ceramic fibers, the innovation of which is that a sol-gel method is adopted, and the specific steps are as follows:
[0038] (1) Preparation of stable sol:
[0039]a. Mix tetrabutyl titanate with chelating agent triethanolamine, and heat to reflux, then add solvent absolute ethanol to fully stir to form a clear sol;
[0040] b. Add the catalysts glacial acetic acid, calcium acetate, and lead acetate trihydrate in sequence to the clear sol, the concentration is controlled at 1mol / L, and reflux and stir in a water bath at 80°C for 1 hour to obtain stable Pb 1-x Ca x TiO 3 (x=0-30%) pale yellow stable sol;
[0041] The molar ratio of calcium acetate to lead acetate trihydrate, glacia...
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