High-efficiency flue gas desulfurization and denitrification catalyst and preparation method thereof
A technology of desulfurization and denitrification and catalyst, which is applied in the field of desulfurization and denitrification, and can solve the problems of high desulfurization and denitrification rate and high operating cost
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[0027] Wherein, the preparation method of graphitized activated carbon comprises the following steps:
[0028] Add iron nitrate and sodium carbonate to activated carbon, heat treatment at 500-1000°C for 5-8 hours in a nitrogen atmosphere, and then wash and dry with 0.4-0.6mol / L dilute nitric acid and distilled water in turn to obtain graphitized activated carbon; activated carbon, nitric acid The mass ratio of iron to sodium carbonate is 1:(0.1-0.2):(0.2-0.3).
[0029] The preparation method of alcohol aminated activated carbon comprises the following steps:
[0030] Add triethanolamine and sodium hydroxide to activated carbon, heat-treat at 500-1000°C for 5-8 hours in a nitrogen atmosphere, and then wash and dry with 0.4-0.6mol / L dilute nitric acid and distilled water in sequence to obtain graphitized activated carbon; activated carbon, The mass ratio of triethanolamine and sodium hydroxide is 1:(0.16-0.22):(0.3-0.4).
[0031] In the embodiment of the present invention, the...
Embodiment 1
[0038] The preparation method of graphitized activated carbon comprises the following steps:
[0039] Add ferric nitrate and sodium carbonate to activated carbon, heat-treat at 750°C for 6.5 hours in a nitrogen atmosphere, and then wash and dry with 0.5mol / L dilute nitric acid and distilled water in turn to obtain graphitized activated carbon; the mixture of activated carbon, ferric nitrate and sodium carbonate The mass ratio is 1:0.15:0.25.
Embodiment 2
[0041] The preparation method of graphitized activated carbon comprises the following steps:
[0042] Add ferric nitrate and sodium carbonate to activated carbon, heat treatment at 1000°C for 8 hours in a nitrogen atmosphere, and then wash and dry with 0.6mol / L dilute nitric acid and distilled water in turn to obtain graphitized activated carbon; the mass of activated carbon, ferric nitrate and sodium carbonate The ratio is 1:0.2:0.3.
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