Preparation method of aging-enhanced copper-chromium alloy
An enhanced and alloyed technology, which is applied in the field of preparation of aging-enhanced CuCr alloys, can solve the problems of Cr agglomeration, large precipitated phase size, and low content, and achieve the effects of good alloy composition uniformity, simple operation, and high density
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[0027] Example 1
[0028] Use a balance to weigh a certain percentage of copper and chromium. The mass ratio of chromium is 4%. The oil and impurities on the surface of the material are removed. The smelting is carried out in a vacuum induction melting furnace with a vacuum of 8×10. -3 Pa, nitrogen protective atmosphere + 0.05MPa, heating rate of 2℃ / s, superheating degree of 200℃, holding time for 5min, and then using restricted nozzle atomization, atomization pressure 5MPa, nozzle diameter 4mm, atomization process is about 9s, right The prepared alloy powder is sieved with different particle sizes, the alloy powder with a certain particle size is cold-pressed, and then the cold-pressed sample is placed in a Φ21 graphite mold for atmosphere protection, hot-press sintering, and the sintering temperature is 1030℃ , The pressure is 30MPa, and the holding time is 1h. After the surface of the hot-pressed sample is treated, the sample is aged at 450℃ for 2h, and the resulting alloy samp...
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[0031] Example 2
[0032] Use a balance to weigh a certain mass fraction of copper and chromium particles, the mass ratio of chromium is 3.5%, remove the oil and impurities on the surface of the material, and smelt in a vacuum induction melting furnace with a vacuum of 9×10 -3 Pa, nitrogen protective atmosphere +0.04MPa, heating rate of 2℃ / s, superheating degree of 200℃, heat preservation for 6min, and then use restricted nozzle atomization, atomization pressure 6MPa, nozzle diameter 4mm, atomization process is about 8s, right The prepared alloy powder is sieved with different particle sizes, 29g of alloy powder is weighed and cold-pressed, and then the cold-pressed sample is placed in a Φ21 graphite mold for atmosphere protection, hot-press sintering, and the sintering temperature is 1030℃. The pressure is 30MPa, and the holding time is 1h. After the surface treatment of the hot-pressed sample, the sample is subjected to 440℃ aging treatment for 2h. The resulting alloy sample has...
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[0033] Example 3
[0034] Use a balance to weigh a certain mass fraction of copper and chromium particles, the mass ratio of chromium is 3.5%, and remove the oil and impurities on the surface of the material, and smelt in a vacuum induction melting furnace with a vacuum of 7×10 -3 Pa, nitrogen protective atmosphere +0.04MPa, heating rate of 2℃ / s, superheat degree of 200℃, heat preservation for 6min, and then use restricted nozzle atomization, atomization pressure 5MPa, nozzle diameter 5mm, atomization process is about 7s, right The prepared alloy powder is sieved with different particle sizes, 29g of alloy powder is weighed and cold-pressed, and then the cold-pressed sample is placed in a Φ21 graphite mold for atmosphere protection and hot-press sintering. The sintering temperature is 1020℃. The pressure is 29MPa, and the holding time is 1h. After the surface of the hot-pressed sample is treated, the sample is aged at 460℃ for 2h. The obtained alloy sample has a density of 97% and...
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