Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A kind of anti-reflection coating liquid and preparation method thereof

A coating solution and anti-reflection technology, applied in the direction of coating, etc., can solve the problems of high refractive index of the film layer, poor anti-reflection effect, non-wear resistance, etc., achieve good film uniformity, increase light transmittance, and reduce costs low effect

Active Publication Date: 2020-03-31
萍乡星弛光电科技有限公司
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when spherical sol particles are used to form a film, if the bonding between the particles is weak, it is conducive to the formation of a porous structure, which can reduce the refractive index to 1.2, but the strength is poor and not wear-resistant; if the bonding between the particles is strong, Although the mechanical properties and wear resistance can be greatly improved, the porous structure is greatly sacrificed, the refractive index of the film layer is high, and the anti-reflection effect is not good.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A kind of anti-reflection coating liquid, its preparation method comprises the following steps:

[0030] (1) Slowly add 6% vinylsilane modified silicone resin dropwise to 10% nano-silica and 15% hollow silica to carry out surface modification treatment;

[0031] Among them, the average particle diameter of nano-silica is 15nm, and the average particle diameter of hollow silica is 25nm;

[0032] After surface modification treatment, the organosilicon modifier is attached to the surface of nano-silica and hollow silica particles, making the combination between the particles stronger.

[0033] (2) 10% nano silicon dioxide and 15% hollow silicon dioxide, 5% oxide, 35% deionized water and 1% hydrochloric acid after the above-mentioned surface modification treatment are added in 28% solvent, at 30 ℃ condition Under reaction 15h;

[0034] The solvent is a mixture of ethanol, isopropanol and ethylene glycol in a volume ratio of 1:2:1;

[0035] The oxide is a mixture of alumi...

Embodiment 2

[0038] A kind of anti-reflection coating liquid, its preparation method comprises the following steps:

[0039] (1) Slowly add 8% epoxy silane modified silicone resin dropwise to 15% nano-silica and 20% hollow silica for surface modification;

[0040] Among them, the average particle diameter of nano-silica is 30nm, and the average particle diameter of hollow silica is 50nm;

[0041] After surface modification treatment, the organosilicon modifier is attached to the surface of nano-silica and hollow silica particles, making the combination between the particles stronger.

[0042] (2) 15% nano silicon dioxide and 20% hollow silicon dioxide, 2% oxide, 30% deionized water and 2% catalyst after the above-mentioned surface modification treatment are added in 23% ethylene glycol diethyl ether, React at 60°C for 10 hours;

[0043] The catalyst is an acid solution in which sulfuric acid and nitric acid are configured at a volume ratio of 1:1;

[0044] The oxide is a mixture of zirc...

Embodiment 3

[0047] A kind of anti-reflection coating liquid, its preparation method comprises the following steps:

[0048] (1) Slowly add 10% silicone oil-modified silicone resin dropwise to 5% nano-silica and 10% hollow silica for surface modification;

[0049] Among them, the average particle diameter of nano-silica is 80nm, and the average particle diameter of hollow silica is 110nm;

[0050] After surface modification treatment, the organosilicon modifier is attached to the surface of nano-silica and hollow silica particles, making the combination between the particles stronger.

[0051] (2) 5% nano silicon dioxide and 10% hollow silicon dioxide, 3% oxide, 40% deionized water and 2% acetic acid after the above-mentioned surface modification treatment are added in 30% butanediol monoethyl ether, React at 80°C for 5h;

[0052] The oxide is a mixture of titanium dioxide and zirconium dioxide at a mass ratio of 1:1.

[0053] (3) After cooling while stirring, the anti-reflection coatin...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
particle sizeaaaaaaaaaa
hardnessaaaaaaaaaa
Login to View More

Abstract

The invention relates to the technical field of glass coating, and concretely relates to an antireflection coating solution and a preparation method thereof. The antireflection coating solution is prepared from 5-20% of nano-silica, 5-20% of hollow silica, 5-15% of an organosilicone modifier, 0-5% of oxide, 10-40% of deionized water, 0.5-2% of a catalyst and 10-30% of a solvent. A film formed on the surface of a glass substrate by the coating solution has a large number of internal pores to facilitate the reduction of the refractive index of the film, so the visible light reflectivity of the glass surface is reduced, and the light transmittance of the glass is improved; and the film formed by the coating solution has very good adhesion with the glass substrate, has good uniformity, and canguarantee the mechanical properties of the film.

Description

technical field [0001] The invention relates to the technical field of glass coating, in particular to an anti-reflection coating solution and a preparation method thereof. Background technique [0002] Anti-reflection coatings are widely used in solar cells, photovoltaic glass, flat panel displays, optical devices and other fields. For the solar cell surface encapsulation glass protective layer, the refractive index of the glass is about 1.52, and the air refraction index is 1, which makes up to 8% of the sunlight irradiated on the glass surface reflected, while the encapsulation glass of the solar cell Anti-reflection coating can effectively reduce the loss of incident light. Moreover, impurities such as water vapor in the air and other suspended dust are easy to adhere to the glass surface, which will further reduce the penetration of sunlight. Therefore, this requires the anti-reflection film on the surface of the battery to have environmental resistance and self-cleani...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C09D1/00C09D7/61C09D7/65C03C17/30
CPCC03C17/009C03C2217/44C03C2217/475C03C2217/476C03C2217/477C03C2217/478C03C2217/732C03C2218/11C09D1/00
Inventor 王先玉周光惠钟少芬
Owner 萍乡星弛光电科技有限公司
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More