Method for preparing graphene through electric arc discharge
An arc discharge and graphene technology, which is applied in the field of graphene preparation by arc discharge method, can solve the problems of difficulty in realizing large-scale preparation of graphene, lack of carbon atoms, poor electrical conductivity, etc., and achieves good flexibility and good crystallinity. , the effect of high yield
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[0018] A method for preparing graphene by arc discharge method, comprising the steps of:
[0019] (1) Preparation of graphene:
[0020] In a water-cooled stainless steel vacuum chamber, graphene was prepared by DC arc discharge method; the pressure was 53200 Pa, the volume ratio of hydrogen gas and nitrogen gas mixture was 1:1, and two high-purity graphite rods with a diameter of 10 mm were used as discharge electrodes; during the whole synthesis process , the electrode spacing is always controlled at about 2 mm by a stepping motor, the discharge current is 120 A, and the discharge process lasts for about 30 minutes;
[0021] (2) Preparation of graphene conductive ink:
[0022] The mixture of graphene and ethyl cellulose prepared by the above DC arc method was added to the mixed solution of terpineol and ethanol; then stirred with a magnetic stirrer for 30 min to obtain a black suspension; finally dispersed with an ultrasonic cleaner for 24 h, Obtain graphene conductive ink;...
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