The invention discloses a preparation method of a high-stability carbon rod for preparing a single-walled
carbon nanotube by arc
discharge, the carbon rod prepared by the method is prepared by a secondary
granulation and gradient
sintering process, and the preparation method comprises the following steps: 1) uniformly mixing
graphite powder (C), micron-sized
nickel powder (Ni),
yttrium oxide (Y2O3), phenolic resin and absolute ethyl
alcohol according to a certain proportion, the mixing method is ball milling; 2)
drying the mixture in a hot air box for secondary
granulation; 3) placing the dried mixture in a square or cylindrical mold for
compression molding to obtain a carbon
ingot; and 4) carrying out gradient
sintering on the pressed and molded carbon
ingot to obtain the carbon rod with good
conductivity. The resistivity is 6.9 E <-4 >
omega.m after
sintering treatment at 900 DEG C, and the resistivity is 3.4 E <-4 >
omega.m after sintering treatment at 1000 DEG C. The gradient sintered carbon rod with good
conductivity has good
conductivity, high
mechanical strength and
machinability, and also has the advantages of simple preparation process flow, low price, strong stability,
batch production and the like. Through secondary
granulation and gradient sintering processes, the prepared carbon rod meets the requirement of arc
discharge for synthesis of a single-walled
carbon nanotube, the conductivity of the obtained carbon rod is obviously changed along with different sintering temperatures, and the yield of the single-walled
carbon nanotube is further influenced.