Composite carbon-based [Mo3S13]<2-> electrochemical hydrogen evolution catalyst and preparation method thereof
A composite carbon and catalyst technology, applied in physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve problems such as low electron transfer efficiency, and achieve improved electrochemical hydrogen evolution characteristics, small electrochemical impedance, Ease of industrial mass production
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Embodiment 1
[0041] The preparation method of carbon-based thirteen sulfur trimolybdenum composite electrochemical hydrogen evolution catalyst, the specific steps are as follows:
[0042] (1) Synthesis of (NH4)2Mo3S13 nH2O
[0043] 1) Dissolve (NH4)6Mo7O24·4H2O in ultrapure water with a mass ratio of 1:5;
[0044] 2) Add ammonium polysulfide solution at a volume ratio of 1:6;
[0045] 3) heating the mixture at 96°C for 1024 hours;
[0046] 4) The obtained product is washed with ultrapure water, alcohol, and carbon disulfide to remove excess S element in sequence. That is, purified trimolybdenum tridesulfide crystals were obtained.
[0047] (2) Preparation of reduced graphene oxide carbon nanotube airgel:
[0048] a) Graphene oxide and carbon nanotubes were mixed with ultrapure water at 1 mg / mL respectively, and ultrasonically treated for 30 minutes;
[0049] b) After mixing the solutions in 1), add ascorbic acid at 1 mL / 0.05 g, and then sonicate for 2 hours.
[0050] c) The sonicated m...
Embodiment 2
[0063] With the preparation method of the carbon-based thirteen sulfur trimolybdenum composite electrochemical hydrogen evolution catalyst described in Example 1, the difference is:
[0064] In the preparation of thirteen sulfur trimolybdenum composite graphene carbon nanotube airgel catalyst, thirteen sulfur trimolybdenum, reduced graphene oxide carbon nanotube airgel combined with N, N-dimethylformamide according to 1mg: 3mg : Mix in proportion of 1mL.
Embodiment 3
[0066] With the preparation method of the carbon-based thirteen sulfur trimolybdenum composite electrochemical hydrogen evolution catalyst described in Example 1, the difference is:
[0067] In the preparation of the tridethiridesulfur trimolybdenum composite graphene carbon nanotube airgel catalyst, the sealing reaction temperature was 250°C, and the reaction time was 15 hours.
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