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Water and oil repellent microcapsule finishing agent and preparation method thereof

A microcapsule finishing, water-repellent and oil-repellent technology, applied in fiber treatment, textiles and papermaking, liquid-repellent fibers, etc., can solve environmental hazards and other problems, achieve good film-forming properties, good heat strong binding effect

Inactive Publication Date: 2018-04-20
INTIME FASHION SUZHOU CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, perfluoroalkyl groups with a carbon chain length equal to or greater than eight carbon atoms will not undergo hydrolysis, photolysis or biodegradation in most environmental condition tests, have persistent environmental inertness and bioaccumulative toxicity, and cause harm to the environment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A water- and oil-repellent microcapsule finishing agent, the finishing agent is spherical or ellipsoidal, with an average particle diameter of 10 μm, and the mass ratio of its core material to wall material is 1:0.7; the core material is made of polyfluoroalkyl Silicon acrylate, butyl acrylate and methyl methacrylate, and the wall material is composed of sericin and chitosan.

[0019] The core material is composed of polyfluoroalkyl silicon acrylate, butyl acrylate and methyl methacrylate in a mass ratio of 3:2:1.

[0020] The wall material is composed of sericin and chitosan in a mass ratio of 3:1.

[0021] A method for preparing a water-repellent and oil-repellent microcapsule finishing agent, comprising the following steps:

[0022] (1) dissolving sericin in deionized water to prepare a sericin solution with a mass concentration of 2%;

[0023] (2) Dissolve chitosan in glacial acetic acid solution, prepare chitosan acetic acid solution with a mass fraction of 1.5%,...

Embodiment 2

[0030] A water and oil repellent microcapsule finishing agent, the finishing agent is spherical or ellipsoidal, with an average particle diameter of 18 μm, and the mass ratio of its core material to wall material is 1:1.2; the core material is made of polyfluoroalkyl Silicon acrylate, butyl acrylate and methyl methacrylate, and the wall material is composed of sericin and chitosan.

[0031] The core material is composed of polyfluoroalkyl silicon acrylate, butyl acrylate and methyl methacrylate in a mass ratio of 5:3:2.

[0032] The wall material is composed of sericin and chitosan in a mass ratio of 4:1.

[0033] A method for preparing a water-repellent and oil-repellent microcapsule finishing agent, comprising the following steps:

[0034] (1) dissolving sericin in deionized water to prepare a sericin solution with a mass concentration of 5%;

[0035] (2) Dissolve chitosan in glacial acetic acid solution, prepare chitosan acetic acid solution with a mass fraction of 3%, th...

Embodiment 3

[0042] A water and oil repellent microcapsule finishing agent, the finishing agent is spherical or ellipsoidal, with an average particle diameter of 25 μm, and the mass ratio of its core material to wall material is 1:1.8; the core material is made of polyfluoroalkyl Silicon acrylate, butyl acrylate and methyl methacrylate, and the wall material is composed of sericin and chitosan.

[0043] The core material is composed of polyfluoroalkyl silicon acrylate, butyl acrylate and methyl methacrylate in a mass ratio of 7:5:3.

[0044] The wall material is composed of sericin and chitosan in a mass ratio of 5:1.

[0045] A method for preparing a water-repellent and oil-repellent microcapsule finishing agent, comprising the following steps:

[0046] (1) dissolving sericin in deionized water to prepare a sericin solution with a mass concentration of 10%;

[0047] (2) Dissolve chitosan in glacial acetic acid solution, prepare chitosan acetic acid solution with a mass fraction of 4.5%,...

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Abstract

The invention discloses a water and oil repellent microcapsule finishing agent and a preparation method thereof. The finishing agent takes the shape of a sphere or ellipsoid, the average particle sizeof the finishing agent is 10-25 [mu]m, and the mass ratio of a core material to a wall material is 1:(0.7-1.8); the core material consists of multi-fluothane silicon acrylate, butyl acrylate and methyl methacrylate; and the wall material consists of sericin and chitosan. The water and oil repellent microcapsule finishing agent disclosed by the invention has the advantages of being high in filmingproperty, high in adhesion property and high in thermal resistance, and a residual liquid generated in the finishing process of the finishing agent disclosed by the invention can be cooled and recycled at a normal temperature, so that environment pollution and raw material waste are avoided.

Description

technical field [0001] The invention belongs to the technical field of textiles and relates to a finishing agent for functional fabrics, in particular to a water- and oil-repellent microcapsule finishing agent and a preparation method thereof. Background technique [0002] Water and oil repellent finishing is a symbol of the continuous development of textile products towards high performance and multifunctionality. The fabrics after water and oil repellent finishing have the characteristics of low surface energy. The importance of this kind of fabrics in the fields of clothing, decoration and industry has been gradually recognized and valued by people. The additives that can impart water and oil repellency to fabrics are mainly fluorine-containing acrylate polymers, which have the characteristics of good film-forming properties, strong adhesion, and UV resistance, and have the advantages of abundant raw material sources and easy production. , but also has the disadvantage o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M23/12D06M13/224D06M13/236D06M15/15D06M15/03
CPCD06M23/12D06M13/2246D06M13/236D06M15/03D06M15/15D06M2200/11D06M2200/12
Inventor 郭新华张会良叶萍韩建钢
Owner INTIME FASHION SUZHOU CO LTD