Test for performance of enhanced ceramic fiber cordierite-prepared oil well anti-water-seepage well cementing test block

A fiber cordierite and reinforced technology, which is applied to the performance test of oil well anti-seepage water cementing test blocks prepared by reinforced ceramic fiber cordierite, in the field of materials, can solve the problems of high water loss, poor impact resistance and poor toughness of test blocks and other problems to achieve the effect of improving pore flow resistance and reducing permeability

Inactive Publication Date: 2018-04-20
ZIBO VOCATIONAL INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, in oil well cementing at home and abroad, cement slurry is used for high temperature and high pressure oil wells, but fly ash floating beads are used, the compressive strength is low, the rate of change of cement slurry density is large, and excessive water loss occurs after the cement slurry is statically solidified. 1. The shrinkage ratio of the test block is too large. In addition, the test block has poor toughness, tensile strength, flexural resistance, and impact resistance, and a large amount of water loss is reduced, resulting in leakage

Method used

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  • Test for performance of enhanced ceramic fiber cordierite-prepared oil well anti-water-seepage well cementing test block

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The performance test of the oil well anti-seepage water cementing test block prepared by reinforced ceramic fiber cordierite includes the following steps:

[0025] Step 1: Preparation of cordierite closed-cell hollow ceramic microbeads: First, the cordierite is crushed into small particles of 1000µm by a jaw crusher, and then made into 70µm spherical solid particles through a Raymond mill, and the spherical solid particles are passed through a lifting The machine enters the dispenser, and then enters the expansion furnace from the dispenser. After expansion at 830°C, firing at 1200°C, and cooling, cordierite closed-cell hollow ceramic microspheres with a wall thickness of 80µm and a particle size of 250µm are formed.

[0026] The second step, the ingredients of the anti-seepage water cementing test block: 43wt% of G-grade oil well cement, 15wt% of ultra-fine cement, 25wt% of cordierite closed-cell hollow ceramic microspheres with a particle size of 250μm, and 1.1% of the...

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Abstract

The invention provides a test for performance of an enhanced ceramic fiber cordierite-prepared oil well anti-water-seepage well cementing test block, wherein the test includes the following steps: preparing materials of an anti-water-seepage well cementing test block: taking 40-50 wt% of G-grade oil well cement, 10-15 wt% of superfine cement, 25-35 wt% of cordierite closed-pore hollow ceramic microbeads with the particle diameter of 50-250 [mu]m, 5-7 wt% of fly ash with loss on ignition of 1.1%, 1.5-2 wt% of calcium oxide with the purity of 99.9%, 0.5-1.0 wt% of sodium sulfate, 1-5 wt% of silica fume and 1.0-2 wt% of an aluminum oxide powder, to obtain a mixture, wherein the sum of the weight percentages of the components is 100%; and slurry-adjusting the obtained mixture with the water-cement ratio of 0.5-0.7 to prepare a slurry, then adding a foaming agent with the amount 0.2-0.5% of the total weight of the mixture, then adding ceramic fibers, graphite microbeads and expansion resinin proportion, stirring evenly, and carrying out anti-water-seepage performance test.

Description

technical field [0001] The invention relates to the performance test of an oil well anti-seepage water cementing test block prepared by reinforced ceramic fiber cordierite, and belongs to the field of material technology. Background technique [0002] At present, in oil well cementing at home and abroad, cement slurry is used for high temperature and high pressure oil wells, but fly ash floating beads are used, the compressive strength is low, the rate of change of cement slurry density is large, and excessive water loss occurs after the cement slurry is statically solidified. 1. The shrinkage ratio of the test block is too large. In addition, the test block has poor toughness, tensile strength, flexural resistance, and impact resistance, and a large amount of water loss is reduced, resulting in leakage. Contents of the invention [0003] Using cordierite material as a lightening agent, adding silica powder and alumina powder, improves the performance of the cementing test...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28G01N11/00G01N9/36G01N5/00G01N15/08
Inventor 冯青
Owner ZIBO VOCATIONAL INST
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