A silver nanocrystal reinforced erbium-doped bismuthate laser glass for optical fiber amplifier and preparation method thereof
A technology of optical fiber amplifier and silver nanocrystal, which is applied in the field of materials science, can solve the problems affecting the local field strength and the luminescence performance of rare earth ions, and achieve the effect of enhancing luminescence performance and uniform physical and chemical properties
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Embodiment 1
[0017] The glass composition is shown in 1# in Table 1, and the specific preparation process is as follows:
[0018] 1) Calculate the quality of each raw material composition according to the mole percentage of the 1# formula glass component in Table 1, weigh the corresponding raw materials, put them into an agate mortar and grind them thoroughly, and mix them evenly;
[0019] 2) Put the uniformly mixed raw materials into a corundum crucible and place them in a silicon carbide rod resistance furnace, and melt them in the range of 1000-1100°C for 15-25 minutes to obtain a molten and clarified glass liquid. The obtained molten and clarified glass liquid Pouring on a preheated (200-250°C) mold;
[0020] 3) After the glass liquid is solidified, quickly put it into a muffle furnace at 350-400°C for annealing, keep it warm for 3-4 hours, and then cool down to room temperature with the furnace to obtain an optically uniform glass.
[0021] The annealed sample was processed into a 20...
Embodiment 2
[0023] Composition is as shown in 2# in table 1, and concrete preparation process is as follows:
[0024] 1) Calculate the quality of each raw material composition according to the mole percentage of the 2# formula glass component in Table 1, weigh the corresponding raw materials, put them into an agate mortar and grind them thoroughly, and mix them evenly;
[0025] 2) Put the uniformly mixed raw materials into a corundum crucible and place them in a silicon carbide rod resistance furnace, and melt them in the range of 1000-1100°C for 15-25 minutes to obtain a molten and clarified glass liquid. The obtained molten and clarified glass liquid Pouring on a preheated (200-250°C) mold;
[0026] 3) After the glass liquid is solidified, quickly put it into a muffle furnace at 350-400°C for annealing, keep it warm for 3-4 hours, and then cool down to room temperature with the furnace to obtain an optically uniform glass.
[0027] The annealed sample was processed into a 20×10×1 mm gl...
Embodiment 3
[0029] Composition is as shown in 3# in table 1, and concrete preparation process is as follows:
[0030] 1) Calculate the quality of each raw material composition according to the molar percentage of the 3# formula glass component in Table 1, weigh the corresponding raw materials, put them into an agate mortar and grind them thoroughly, and mix them evenly;
[0031] 2) Put the uniformly mixed raw materials into a corundum crucible and place them in a silicon carbide rod resistance furnace, and melt them in the range of 1000-1100°C for 15-25 minutes to obtain a molten and clarified glass liquid. The obtained molten and clarified glass liquid Pouring on a preheated (200-250°C) mold;
[0032] 3) After the glass liquid is solidified, quickly put it into a muffle furnace at 350-400°C for annealing, keep it warm for 3-4 hours, and then cool down to room temperature with the furnace to obtain an optically uniform glass.
[0033] The annealed sample was processed into a 20×10×1 mm g...
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