Preparation technology of Yishen granules
A preparation process and granule technology, applied in the field of preparation of Yishen granules, can solve problems such as loss of effective components, and achieve the effects of improving effective active components, avoiding a large amount of loss, and avoiding loss.
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Embodiment 1
[0019] A preparation process for Yishen Granules, comprising the steps of:
[0020] Take 250g of fermented Cordyceps powder, 250g of Ganoderma lucidum, and 50g of medlar;
[0021] Take the fermented Cordyceps fungus powder, add 5 times the weight of water, soak for 30 minutes, extract the volatile oil by distillation, extract for 3 hours, collect the volatile oil, then add absolute ethanol accounting for twice the volume of the raffinate to the raffinate, and reflux to extract two 2 hours for the first extraction and 1 hour for the second extraction. During the extraction process, the temperature is controlled at 50°C and the microwave power is 500W. Filter separately, combine the filtrates, recover ethanol by vacuum rotary evaporation, and then concentrate to 1.35-1.40g / ml of extract, finally mixed with volatile oil to obtain component A;
[0022] Crush Ganoderma lucidum, then grind it into fine powder, pass through a 200-mesh sieve, spread it into a flat layer with a thick...
Embodiment 2
[0027] A preparation process for Yishen Granules, comprising the steps of:
[0028] Take 250g of fermented Cordyceps powder, 250g of Ganoderma lucidum, and 50g of medlar;
[0029] Fermented Cordyceps powder was extracted twice with 60% ethanol, each time adding 8 times the amount of 60% ethanol, each time for 12 hours, combined the extracts, filtered, and the filtrate was decompressed to recover ethanol, then concentrated under reduced pressure to a density of 1.20~ 1.25g / ml clear paste; decoct Ganoderma lucidum with water twice, add 8 times the amount of water each time, decoct for 2 hours for the first time, and decoct for 1.5 hours for the second time, combine the decoction, filter, and concentrate the filtrate under reduced pressure to Clear ointment with a density of 1.05~1.10g / ml; Lycium barbarum is extracted twice with 70% ethanol, each time adding 5 times the amount of 70% ethanol, each time for 48 hours, the filtrate is combined, filtered, and the filtrate is decompre...
Embodiment 3
[0032] The extraction process of comparative example 1-2: compared with embodiment 2, the adenosine content in the product of embodiment 1 has improved by 11.3%, mannitol has improved by 6.7%, wolfberry polysaccharide has improved by 23.9%, sterol, saponin, amino acid Active components such as fritillaria and fritillary base substances are also greatly improved; after testing, the content of Ganoderma lucidum polysaccharides in component B of Example 1 is 913.4mg, and the content of Ganoderma lucidum polysaccharides in the Ganoderma lucidum extract clear paste of Example 2 is 607.2mg, Increased by 50%.
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