A kind of preparation method of coal-saving agent
A technology of coal-saving agent and surfactant, which is applied in the field of preparation of coal-saving agent, can solve the problems of large addition amount, pollute the environment, etc. Effect
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[0024] A preparation method of a coal-saving agent, the preparation method comprising the steps of:
[0025] (1) According to the mass ratio of 1:5, mix the multi-walled carbon nanotubes and chitosan solution, and ultrasonically oscillate at a temperature of 70-80°C for 3-4 hours to obtain the oscillation liquid. According to the mass ratio of 10-15:1, Mix the alcohol aqueous solution and the surfactant, and stir evenly to obtain a mixed solution;
[0026] (2) In terms of parts by weight, take 40~50 parts of mixed solution, 10~15 parts of ethanol solution, 5~6 parts of oscillating solution, and 1~2 parts of butyl titanate, and add the oscillating solution to the mixed solution for ultrasonic dispersion 1 For ~2 h, add butyl titanate and ethanol solution under stirring at 200~300r / min at a temperature of 28~32°C, let it stand for 4~5 h, filter to obtain a filter residue, and dry the filter residue at a temperature of 100~120°C for 3~ 4h, and then roasted at a temperature of 10...
Embodiment 1
[0031] Multi-walled carbon nanotubes were purchased from Beijing Deke Daojin Technology Co., Ltd.
[0032] Chitosan solution is to mix chitosan and acetic acid solution according to the mass ratio of 1:5, and stir evenly to obtain chitosan solution.
[0033] The alcohol aqueous solution is to mix ethanol and water evenly according to the mass ratio of 1:0.8 to obtain the alcohol aqueous solution.
[0034] The surfactant was cetyltrimethylammonium bromide.
[0035] Gases are nitrogen, carbon dioxide, oxygen.
[0036] The cleaning agent is cyclopentadiene.
[0037] A preparation method of a coal-saving agent, the preparation method comprising the steps of:
[0038](1) According to the mass ratio of 1:5, mix the multi-walled carbon nanotubes and chitosan solution, and ultrasonically oscillate for 3 hours at a temperature of 70°C to obtain the oscillation liquid. The agent is mixed, stirred evenly, and a mixed solution is obtained;
[0039] (2) In parts by weight, take 40 par...
Embodiment 2
[0044] Multi-walled carbon nanotubes were purchased from Beijing Deke Daojin Technology Co., Ltd.
[0045] Chitosan solution is to mix chitosan and acetic acid solution according to the mass ratio of 1:5, and stir evenly to obtain chitosan solution.
[0046] The alcohol aqueous solution is to mix ethanol and water evenly according to the mass ratio of 1:0.8 to obtain the alcohol aqueous solution.
[0047] The surfactant is sodium lauryl sulfate.
[0048] Gases are nitrogen, carbon dioxide, oxygen.
[0049] The cleaning agent is cyclopentadiene.
[0050] A preparation method of a coal-saving agent, the preparation method comprising the steps of:
[0051] (1) Mix multi-walled carbon nanotubes and chitosan solution at a mass ratio of 1:5, and ultrasonically oscillate at a temperature of 75°C for 3 hours to obtain an oscillation solution. The agent is mixed, stirred evenly, and a mixed solution is obtained;
[0052] (2) In terms of parts by weight, take 45 parts of mixed solu...
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