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437results about How to "Not easy to dissolve" patented technology

Preparation method of high-viscosity organic silicon defoamer

InactiveCN104069654AIncrease the molecular chain lengthGood defoaming performanceFoam dispersion/preventionRoom temperatureOil phase
The invention discloses a preparation method of a high-viscosity organic silicon defoamer. The preparation method comprises the following steps of preparing a silicon grease by using organopolysiloxane, dewatering particles, catalysts and silicon resin under 180-240 DEG C, and stirring and uniformly mixing the silicon grease, polyether modified silicone oil and an emulsifying agent under 72-78 DEG C so as to obtain an oil phase mixture, dissolving a dispersing thickening agent in water; then adding a sodium hydroxide solution to uniformly stir to obtain emulsifying thickening water, adding the emulsifying thickening water into an oil-phase mixture, and carrying out emulsifying stir on the oil-phase mixture under 72-78 DEG C to obtain a coarse emulsifying object; and homogenizing the coarse emulsifying object under 50-55 DEG C to obtain a fine emulsifying object, adding residue water into the fine emulsifying object, stirring and uniformly mixing the fine emulsifying object under room temperature so as to obtain the high-viscosity organic silicon defoamer. The preparation method provided by the invention has the advantages that high-viscosity simethicone is utilized as an emulsifying main raw material, and thus, the obtained high-viscosity organic silicon defoamer has an ultra-strong defoaming speed and an anti-foam effect.
Owner:道尔达(西安)新材料有限公司

Cathode material of lithium ion battery and preparation method of cathode material

The invention discloses a cathode material of a lithium ion battery. The cathode material has an atomic ratio of LiaMxMn(2-x)O(4-y)Zy. Primary particles of the cathode material of the lithium ion battery are substantially spherical, and the surface of each primary particle consists of 2 to 120 multilayer crystal dislocation frustums. The invention provides a preparation method of the cathode material of the lithium ion battery. The cathode material of the lithium ion battery is prepared by annealing, cooling and grinding a lithium manganate precursor in a roasting treatment mode of repeatedly changing roasting temperature. The invention has the advantages that by repeatedly changing the roasting temperature in the roasting process, the prepared cathode material of the lithium ion battery has a dislocation structure, and the mobility of ions and electrons from the inner part of the material to the outer part of the material is improved, and the magnification performance of a lithium manganate material is improved. Because the cathode material is substantially spherical, the specific surface area of the lithium manganate material is reduced, and manganese is difficult to dissolve, so the cathode material of the lithium ion battery is high in high-temperature cycle performance.
Owner:宁波富理电池材料科技有限公司

Preparation process of hydrogen fuel battery membrane electrode

The invention discloses a preparation process of a hydrogen fuel battery membrane electrode, and belongs to the field of battery membrane electrodes. The membrane electrode is prepared by the aid of an ultrasonic spraying process and a heat transfer printing process. The preparation process includes the steps: firstly, sequentially spraying a transfer printing medium with carbon powder slurry, electric catalyst slurry and binding agent slurry by the aid of the ultrasonic spraying process; secondly, loading a catalyst layer on a proton exchange membrane by the aid of the heat transfer printing process; finally, performing hot-pressing for self-made diffusion layers by the aid of the ultrasonic spraying process to obtain the membrane electrode. According to the preparation process, the diffusion layers are closely combined by the aid of actions among Nafion slurry, the proton exchange membrane and carbon powder slurry and the diffusion layers, electrochemical performance of the membrane electrode is greatly improved by the aid of the heat transfer printing process, the service life of the membrane electrode is prolonged, the problems such as wrinkle and swelling of the proton exchange membrane are solved, a lot of time for paving and treating the membrane is saved, and mass production of the membrane electrode is facilitated.
Owner:KUSN INNOVATION INST OF NANJING UNIV

Method for preparing sustained-release fertilizer

The invention relates to a method for preparing a sustained-release fertilizer, and belongs to a method for preparing the sustained-release fertilizer by embedding a fertilizer into the pores of a carrier, in particular a method for preparing the sustained-release fertilizer by embedding the fertilizer into the pores of porous microspheres puffed by mountain flour in a larger amount than that in the prior art. The method comprises the following steps of: putting the porous microspheres puffed by the mountain flour in a vacuum container which is vacuumized; stopping vacuumizing after the air in the pores of the porous microspheres puffed by the mountain flour is pumped out completely; pouring the fertilizer into the vacuum container; uniformly mixing the porous microspheres puffed by the mountain flour and the fertilizer; gradually reducing the vacuum to normal pressure to ensure that the fertilizer is absorbed into the pores of the porous microspheres puffed by the mountain flour as much as possible; and thus, obtaining a sustained-release fertilizer primary product. Compared with the method of simply mixing the porous microspheres puffed by the mountain flour and the fertilizer, the method not only increases the vacuumization process and the cost, but prolongs the utilizable time of the fertilizer in the soil, increases the utilization rate of the fertilizer and reduces the fertilizer pollution.
Owner:河北硅谷肥业有限公司

Method for recovering bismuth from bismuth slag

The invention relates to a method for recovering bismuth from bismuth slag, which includes steps of: firstly, smelting silver-refining converter oxidizing slag in high-temperature restoring mode to obtain lead-bismuth alloy, performing silico-fluoric acid system lead-bismuth alloy electrolysis to obtain electric lead products and high-bismuth anode mud; secondly performing hydrochloric acid leaching on the high-bismuth anode mud, filtering to obtain bismuth-contained leaching liquid, wherein the leaching condition is that: liquid-solid ratio (weight ratio) is 3-6:1, process temperature is 40-70 DEG C, hydrochloric acid concentration is 150-200g / L, and reaction time is1.5-2.5h; and thirdly, replacing bismuth in the leaching liquid through reduced iron powder to obtain sponge bismuth and obtain refined bismuth with high purity in pyro-refining electrolysis. Sodium sulfide for sedimenting silver is added in the leaching process to obtain bismuth leaching liquid, silver can be prevented from immersing into the liquid as much as possible, when return washing liquid is used for leaching high-bismuth anode mud, a part of hydrochloric acid is refilled to maintain necessary potential of hydrogen (pH) value, concentration of Cl- is controlled to be 150-200g / L, and simultaneously bismuth ion hydrolysis can be avoided. Compared with the prior art, the method has no operations of water quenching, ball milling, hydrolysis, neutralization and the like of coarse bismuth alloy, has less procedures, is low in cost and free of pollution, simultaneously achieves double-metal electrolysis of the lead-bismuth alloy and does not influence the electric-lead main system.
Owner:蒙自矿冶有限责任公司

Multi-enzyme complex preparation containing microcapsule and preparation method and application thereof

Provided are a multi-enzyme complex preparation containing microcapsule and a preparation method and an application thereof. The preparation method includes placing 20.7%-22.9% of amylase, 8.4%-11.3% of saccharifying enzyme, 7.6%-9.8% of cellulose, 10.9%-13.1% of pectinase, 11.4%-15.3% of catalase, 6.4%-9.7% of laccase, 0.2%-8.5% of enzyme stabilizer and 0.01%-0.5% of preservative by weight into water, stirring the mixture to enable the mixture to be dissolved completely and form water solution, dispersing 8.6%-12.5% of microencapsulation protease into the water solution to obtain the multi-enzyme complex preparation containing the microcapsule. The multi-enzyme complex preparation containing the microcapsule is added into tobacco raw materials in a feeding mode according to 0.5%-1% of the weight of the tobacco raw materials in a tobacco threshing re-baking line or a tobacco storage alcoholization or formula tobacco thread making line. The microencapsulation protease in the multi-enzyme complex preparation contains a high polymer material wall material, the protease wrapped by the wall material is not easy to dissolve in the low water solution state and can be dispersed and dissolved quickly in the diluted high water solution state, so that activity loss of the protease and other enzymes caused by the fact that the protease reacts with other enzymes is avoided.
Owner:YUNNAN REASCEND TOBACCO TECH GRP

Composite medicine coating balloon, preparation method thereof, and composite medicine coating balloon dilatation catheter

The invention discloses a composite medicine coating balloon. The composite medicine coating balloon comprises a balloon body and a composite medicine coating covering the surface of the balloon body,wherein the composite medicine coating comprises a bottom-layer coating, a middle-layer coating and an outer-layer coating; the bottom-layer coating is used for coating the surface of the balloon body, and consists of medicines A and a hydrophilic excipient; the middle-layer coating consists of a medicine B packed with a packing agent and hydrophilic excipients / lipophilic excipients / amphipathic excipients; and the outer-layer coating consists of a medicine C and lipophilic excipients / amphipathic excipients. The invention further discloses a preparation method of the composite medicine coatingballoon and a composite medicine coating balloon dilatation catheter. According to the composite medicine coating balloon, the loss of traditional Chinese medicines in the balloon transporting process can be reduced, besides, the vasculopathy position can have effective medicine concentration within a short term, vascular restenosis is restrained, long-time medicine release can be provided, durable medicine action time can be maintained, and the restenosis rate can be reduced.
Owner:KOSSEL MEDTECH SUZHOU

Sustained-release pesticide fertilizer granula and production method thereof

The invention relates to the technical field of pesticide preparations and specifically relates to a sustained-release pesticide fertilizer granula and a production method thereof. The pesticide fertilizer granula is prepared from a sustained-release coating layer and an inner effective matter, wherein the sustained-release coating layer is prepared from talcum powder, neutral bentonite, hydroxymethyl cellulose and chitosan which are mixed according to the mass ratio of 8 to 5 to 2 to 1; the effective matter is prepared from sustained-release medicine, compound fertilizer, a wetting expandingagent and a filling agent; the sustained-release medicine is a coated systematic type pharmaceutical preparation; the systematic type pharmaceutical preparation and a mesoporous AcF micro powder carrier are mixed and then coated; a coating material is prepared from the following ingredients of polyglycolic acid, talcum powder, mesoporous silica, cyclodextrin, liquid paraffin, polyvinyl alcohol, calcium dodecyl benzene sulfonate and deionized water. The pesticide fertilizer granula is treated by a special coating technology, has the characteristics of quick and stable fertilizer efficiency andslow and durable insect killing pesticide effect and is suitable for synchronous pesticide fertilizer application of flowers and nursery stock plants.
Owner:JIXI NONGHUA BIOTECH
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