Negative pole active material and preparation method thereof, negative pole piece and battery core
A negative electrode active material and negative electrode sheet technology, applied in the direction of circuits, electrical components, battery electrodes, etc., can solve the problems of few applications in the field of consumer electronics, low charge and discharge capacity of lithium titanate, limited energy density, etc., to achieve superior Effect of electronic conductivity, improvement of safety performance of hot box, and high oxygen reduction activity
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[0020] Next, the preparation method of the negative electrode active material according to the second aspect of the present invention is described, which is used to prepare the negative electrode active material described in the first aspect of the present invention, comprising the steps of: (1) dissolving the lanthanum salt, the strontium salt, and the manganese salt respectively in the and mixed in ionic water to form a mixed solution; (2) adding a chelating agent and a buffer to the mixed solution for gelation reaction to obtain a lanthanum strontium manganese oxygen wet gel; (3) adding titanium to the lanthanum strontium manganese oxygen wet gel Lithium oxide powder, then dried and sintered to complete the preparation of the negative electrode active material, wherein the obtained negative electrode active material includes a lithium titanate core and a coating layer coated on the surface of the lithium titanate core, the coating The coating is selected from lanthanum stron...
Embodiment 1
[0042] (1) Preparation of negative electrode sheet
[0043] Lanthanum nitrate, strontium nitrate, and manganese nitrate are dissolved in deionized water according to the molar ratio of La, Sr, and Mn of 0.7:0.3:1, and a mixed solution with a total ion concentration of La, Sr, and Mn of 1mol / L is prepared, and then Add citric acid (the ratio of the moles of citric acid to the sum of La, Sr, and Mn ion moles is 2.5:1) and ammonium bicarbonate for gelation reaction to obtain lanthanum strontium manganese oxygen wet gel, wherein the reaction temperature The temperature is 80°C, the pH of the reaction system is 3, and the reaction time is 5h-10h. According to the coating ratio of 0.1% (that is, the quality of the finally obtained lanthanum strontium manganese oxide is 0.1% of the mass of lithium titanate), add commercial lithium titanate powder to the lanthanum strontium manganese oxide wet gel, and then bake dry, and after the solvent deionized water is fully volatilized, the obt...
Embodiment 2
[0052] A lithium-ion battery was prepared according to the method of Example 1, with the difference that: the coating ratio was 0.5%, and the thickness of the coating layer was about 0.15 μm.
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