Method for preparing dioctyl phosphine oxide
A technology of dioctylphosphine oxide and dioctylphosphine chloride, which is applied in the field of phosphorus chemical industry, can solve the problems of production method toxicity, high operation difficulty, and low yield, and achieve high product purity, good atom economy, and reaction Effects in simple steps
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Embodiment 1
[0022] Dioctylphosphorus chloride was added to distilled water at room temperature, stirred and hydrolyzed for 10 minutes, adjusted to pH > 13 with 5wt% NaOH solution, extracted with chloroform, the organic layer was taken, washed with distilled water until neutral, and evaporated to remove the organic layer by a rotary evaporator. layer solvent, dissolved in acetic acid, filtered, and the filter residue was discarded, adding chloroform and distilled water to extract the filtrate, collecting the organic layer, washing with distilled water until neutral, and drying in vacuo to obtain a white solid with a yield of 98%.
Embodiment 2
[0024] Dioctylphosphorus chloride was added to distilled water at room temperature, stirred and hydrolyzed for 30 minutes, adjusted to pH > 13 with 15wt% NaOH solution, extracted with chloroform, and the organic layer was taken, washed with distilled water until neutral, and evaporated by a rotary evaporator to remove the organic layer. layer solvent, dissolved in acetic acid, filtered, and the filter residue was discarded, added chloroform and distilled water to extract the filtrate, collected the organic layer, washed with distilled water until neutral, and dried in vacuo to obtain a white solid with a yield of 98.5%.
Embodiment 3
[0026] Dioctylphosphorus chloride was added to distilled water at room temperature, stirred and hydrolyzed for 20 minutes, adjusted to pH > 13 with 10wt% NaOH solution, extracted with chloroform, and the organic layer was taken, washed with distilled water until neutral, and evaporated by a rotary evaporator to remove the organic layer. layer solvent, dissolved in acetic acid, filtered, and the filter residue was discarded, adding chloroform and distilled water to extract the filtrate, collecting the organic layer, washing with distilled water until neutral, and drying in vacuo to obtain a white solid with a yield of 99%.
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