Light halogen-free flame-retardant reinforced polyamide composition and preparation method thereof
A polyamide composition and polyamide technology, applied in the field of lightweight halogen-free flame-retardant reinforced polyamide composition and its preparation, can solve the problems of many defects and poor performance
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Embodiment 1
[0087] Polyamide 56 (PA56, the relative viscosity of sulfuric acid is 2.72): 3085g
[0088] Flame retardant melamine cyanurate: 350g
[0089] Flame retardant synergist zinc borate: 150g
[0090] E-glass fiber: 1000g
[0091] Hollow glass microspheres (particle size 56μm, true density 0.32g / cm 3 , Compression 13.78MPa): 250g
[0092] Compatibilizer methyl methacrylate-butadiene-styrene copolymer MBS: 100g
[0093] Coupling agent KH-550: 2.5g
[0094] Other additives combination (including EBS, calcium stearate, silicone powder, calcium montanate, talc, antioxidant 1098): 62.5g
[0095] The preparation method of light-weight halogen-free flame-retardant reinforced polyamide 56 resin:
[0096] (1) Disperse 50g of coupling agent KH-550 in 150g of ethanol-water (mass ratio 1:1), and then evenly spray the mixed solution on the surface of hollow glass microspheres under high-speed stirring, so that the coupling agent can be evenly coated Cover hollow glass microspheres; the sp...
Embodiment 2
[0107] Polyamide 56 (PA56, the relative viscosity of sulfuric acid is 2.72): 2332.5g
[0108] Flame retardant melamine cyanurate: 350g
[0109] Flame retardant synergist phenoxycyclotriphosphazene: 150g
[0110] E-glass fiber: 1500g
[0111] Hollow glass microspheres (particle size 56μm, true density 0.32g / cm 3 , Compression 13.78MPa): 500g
[0112] Compatibilizer MBS: 100g
[0113] Coupling agent KH-550: 5g
[0114] Other additives combination (including EBS, calcium stearate, silicone powder, calcium montanate, talc, antioxidant 1098): 62.5g
[0115] See Example 1 for sample preparation and testing procedures. See Table 1 for relevant test results.
Embodiment 3
[0117] Polyamide 56 (PA56, the relative viscosity of sulfuric acid is 2.72): 1580g
[0118] Flame retardant melamine cyanurate: 350g
[0119] Flame retardant synergist triphenyl phosphate: 150g
[0120] E-glass fiber: 2000g
[0121] Hollow glass microspheres (particle size 56μm, true density 0.32g / cm 3 , Compression 13.78MPa): 750g
[0122] Compatibilizer MBS: 100g
[0123] Coupling agent KH-550: 7.5g
[0124] Other additives combination (including EBS, calcium stearate, silicone powder, calcium montanate, talc, antioxidant 1098): 62.5g
[0125] See Example 1 for sample preparation and testing procedures. See Table 1 for relevant test results.
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