Production method of super-strength chinlon 66 fiber
A production method and ultra-high-strength technology, applied in the field of spinning, to achieve the effects of reducing crystallization and orientation, uniform and stable viscosity, and accelerating wind speed
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Embodiment 1
[0026] A kind of production method of ultra-high-strength nylon 66 fiber, comprises the following steps:
[0027] (1) Polymerization: Nylon 66 salt solution with a concentration of 52% by mass is concentrated and polymerized to obtain a high-viscosity polymerized spinning melt in a molten state, and the relative viscosity of formic acid of the high-viscosity polymerized spinning melt is 80 ;
[0028] (2) Spinning: The high-viscosity polymerized spinning melt is transported to the spinning box through the melt pipeline, quantitatively pressed into the spinning assembly by the metering pump, and then sprayed out from the spinneret to form a tow in the spinning box; Wherein, the temperature of the melt pipeline is 290°C; the temperature of the spinning box is 315°C; the residence time of the high-viscosity polymer spinning melt in the spinning assembly is 2min; the metering pump is a In-one-out type; the number of holes in the spinneret is 160 holes / plate, the hole spacing is 8....
Embodiment 2
[0035] A kind of production method of ultra-high-strength nylon 66 fiber, comprises the following steps:
[0036] (1) Polymerization: Nylon 66 salt solution with a mass percent concentration of 48% is concentrated and polymerized to obtain a high-viscosity polymerized spinning melt in a molten state, and the relative viscosity of formic acid of the high-viscosity polymerized spinning melt is 76 ;
[0037](2) Spinning: The high-viscosity polymerized spinning melt is transported to the spinning box through the melt pipeline, quantitatively pressed into the spinning assembly by the metering pump, and then sprayed out from the spinneret to form a tow in the spinning box; Wherein, the temperature of the melt pipeline is 295°C; the temperature of the spinning box is 325°C; the residence time of the high-viscosity polymer spinning melt in the spinning assembly is 1.5min; the metering pump is One inlet and four outlets; the number of holes in the spinneret is 104 holes / plate, the hol...
Embodiment 3
[0044] A kind of production method of ultra-high-strength nylon 66 fiber, comprises the following steps:
[0045] (1) Polymerization: Nylon 66 salt solution with a concentration of 55% by mass is concentrated and polymerized to obtain a high-viscosity polymerized spinning melt in a molten state, and the relative viscosity of formic acid of the high-viscosity polymerized spinning melt is 85 ;
[0046] (2) Spinning: The high-viscosity polymerized spinning melt is transported to the spinning box through the melt pipeline, quantitatively pressed into the spinning assembly by the metering pump, and then sprayed out from the spinneret to form a tow in the spinning box; Wherein, the temperature of the melt pipeline is 285°C; the temperature of the spinning box is 305°C; the residence time of the high-viscosity polymer spinning melt in the spinning assembly is 2.5min; the spinneret The number of holes is 230 holes / plate, the hole spacing is 7.5mm, the hole diameter is 0.2mm, and the ...
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