TiZrVHf quaternary getter thin film and preparation method thereof
A getter thin film and thin film technology, applied in ion implantation plating, metal material coating process, coating, etc., can solve the problems of small conductance, unsatisfactory particle accelerator, high secondary electron emission coefficient, etc., and achieve long-term Effects of service life, reduction of secondary electron emission coefficient, and improvement of operating efficiency
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Embodiment 1
[0034] Embodiment 1, the preparation method of TiZrVHf quaternary getter film of the present invention comprises the following steps:
[0035] 1) pretreat the substrate pipeline;
[0036] 2) The pretreated substrate pipe is subjected to pulsed magnetron sputtering, the deposition temperature is 90°C, the Kr flow rate is 2sccm, the sputtering power is 60W, the gas pressure is 1Pa, and the deposition time is 50min, so that Ti, Zr, V, and Hf are formed on the substrate pipe. Dense layer of four elements;
[0037] 3) The substrate obtained in step 2) is subjected to DC magnetron sputtering, the deposition temperature is 150°C, the Kr flow rate is 2sccm, the sputtering power is 100W, the gas pressure is 1Pa, and the deposition time is 300min, so that Ti, Zr, V, and Hf are formed on the substrate pipeline. Columnar layers of four elements.
Embodiment 2
[0038]Embodiment 2, the preparation method of TiZrVHf quaternary getter film of the present invention, comprises the following steps:
[0039] 1) Pretreat the substrate pipeline;
[0040] 2) The pretreated substrate pipe is subjected to pulsed magnetron sputtering, the deposition temperature is 85°C, the Kr flow rate is 4 sccm, the sputtering power is 80W, the gas pressure is 1.2Pa, and the deposition time is 70min, so that Ti, Zr, V, Dense layer of four elements of Hf;
[0041] 3) The substrate obtained in step 2) is subjected to DC magnetron sputtering, the deposition temperature is 200°C, the Kr flow rate is 8sccm, the sputtering power is 80W, the gas pressure is 1.5Pa, and the deposition time is 600min, so that Ti, Zr, V, A columnar layer of the four elements Hf.
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