A kind of preparation method of porous graphene powder for automobile alloy material
A technology of porous graphene and alloy materials, applied in the field of automobile alloy materials, can solve the problems of easily broken hollow glass microbeads, low degree of freedom in structural design, general forming processability, etc., and achieves a simple and easy preparation method and a degree of environmental protection in the process. High, preventing agglomeration problems
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Embodiment 1
[0039] A preparation method for porous graphene powder for automobile alloy materials, comprising the following steps:
[0040] Step 1, adding graphene oxide to absolute ethanol, then adding polyvinylpyrrolidone, and ultrasonically stirring until completely dispersed to obtain a graphene oxide dispersion;
[0041] Step 2, adding the graphene oxide dispersion liquid into a sealed reaction kettle, pressurizing and heating for 1 hour, and gradually lowering the pressure and lowering the temperature for the reaction to obtain mixed graphene oxide;
[0042] Step 3, adding the mixed graphene oxide into the aluminum chloride solution, then stirring and feeding ammonia gas until no precipitation occurs, drying after filtering to obtain the composite graphene oxide precipitate coated with aluminum hydroxide;
[0043] Step 4, adding the composite graphene oxide precipitate into the organic solvent for aeration reaction for 1 hour, then taking it out and drying to obtain the graphene oxi...
Embodiment 2
[0056] A preparation method for porous graphene powder for automobile alloy materials, comprising the following steps:
[0057] Step 1, adding graphene oxide to absolute ethanol, then adding polyvinylpyrrolidone, and ultrasonically stirring until completely dispersed to obtain a graphene oxide dispersion;
[0058] Step 2, adding the graphene oxide dispersion liquid into a sealed reaction kettle, pressurizing and heating for 3 hours, and gradually lowering the pressure and lowering the temperature for the reaction to obtain mixed graphene oxide;
[0059] Step 3, adding the mixed graphene oxide into the aluminum chloride solution, then stirring and feeding ammonia gas until no precipitation occurs, drying after filtering to obtain the composite graphene oxide precipitate coated with aluminum hydroxide;
[0060] Step 4, adding the composite graphene oxide precipitate into an organic solvent for aeration reaction for 3 hours, then taking it out and drying to obtain the graphene ox...
Embodiment 3
[0073] A preparation method for porous graphene powder for automobile alloy materials, comprising the following steps:
[0074] Step 1, adding graphene oxide to absolute ethanol, then adding polyvinylpyrrolidone, and ultrasonically stirring until completely dispersed to obtain a graphene oxide dispersion;
[0075] Step 2, adding the graphene oxide dispersion liquid into a sealed reaction kettle, pressurizing and heating for 2 hours, and gradually lowering the pressure and lowering the temperature for the reaction to obtain mixed graphene oxide;
[0076] Step 3, adding the mixed graphene oxide into the aluminum chloride solution, then stirring and feeding ammonia gas until no precipitation occurs, drying after filtering to obtain the composite graphene oxide precipitate coated with aluminum hydroxide;
[0077] Step 4, adding the composite graphene oxide precipitate into an organic solvent for aeration reaction for 2 hours, then taking it out and drying to obtain the graphene ox...
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