A transfer method of uniform graphene film
A technology of graphene film and transfer method, which is applied in the direction of graphene, chemical instruments and methods, nano-carbon, etc., can solve the problem of not meeting the high conductivity requirements of transparent electrodes, the influence of transparent electrode uniformity and conductivity, and the graphene surface Problems such as uneven resistance, to avoid graphene gaps, good flatness, and low cost
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[0020] The technical solutions of the present invention will be further described below in conjunction with specific examples:
[0021] A transfer method of a uniform graphene film, comprising the steps of:
[0022] (1) The surface of the 25 um thick copper foil is grown by chemical vapor deposition to obtain continuous graphene, and the spin coating concentration of the graphene surface is 100 mg / ml PMMA, and after the spin coating, it is placed on the constant temperature table in 170. Bake at ° C for 5 min;
[0023] (2) After grilling, the unfrotted PMMA is placed in a plasma washing machine to treat 1min, remove graphene on the back copper foil, then plasticizing the PMMA / graphene / copper foil in the concentration of 5 mol / L. FECL 3 The copper foil is etched in the solution, etching 30 min, then transferred to the deionized water for 10 min, then transferred to the new 5 mol / L of FeCl 3 The residual copper foil is etched in the solution, etching 2 h, removes the floc ...
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