Preparation method of antibacterial non-woven cloth and antibacterial non-woven cloth
A technology of non-woven fabrics and polylactic acid fibers, applied in the field of non-woven fabrics, can solve the problems of polylactic acid fibers with high hardness, insufficient softness, and poor hand feeling of non-woven fabrics, and achieve antibacterial performance improvement, content reduction, and hydrophilic sex good effect
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Embodiment 1
[0027] The preparation method of embodiment 1 antibacterial nonwovens comprises the following steps:
[0028] S1, hydrophilic modification of polylactic acid fibers in a mixed solution of water and lipase to obtain hydrophilic polylactic acid fibers;
[0029] S2: The hydrophilic polylactic acid fiber is immersed in a grafting treatment solution containing nanocrystalline cellulose, an esterification catalyst, and an ionic liquid for grafting reaction to obtain a cellulose-grafted polylactic acid fiber;
[0030] S3: Laying cellulose-grafted lactic acid fibers into a single component, fiber web, or blending cellulose-grafted lactic acid fibers with second fibers to form a mixed fiber web, spunlace, washing and drying, to obtain antibacterial non-toxic Finished woven cloth.
[0031] The lipase in S1 is porcine pancreatic lipase L3126, and the composition of S1 mixed solution comprises lipase and disodium hydrogen phosphate-potassium dihydrogen phosphate buffer solution, and the ...
Embodiment 2
[0037] Embodiment 2 is based on Example 1, the difference is that the lipase in S1 is porcine pancreatic lipase L3126, and the composition of S1 mixed solution comprises lipase and disodium hydrogen phosphate-potassium dihydrogen phosphate buffer solution, disodium hydrogen phosphate-phosphoric acid The pH value of potassium dihydrogen buffer solution is 7.7; the technological conditions of S1 hydrophilic modification are: reaction temperature 43°C, reaction time 12h, lipase L3126 concentration 0.3g / L.
Embodiment 3
[0039] The difference between Example 3 and Example 2 is that the ionic liquid is 1-butyl-3-imidazole carboxylate.
[0040] The weight percentage of nanocrystalline cellulose in the grafting treatment liquid is 2%, and the weight percentage of the esterification catalyst in the grafting treatment liquid is 1%.
[0041] The technological conditions of the grafting reaction in S2 are: the reaction temperature is 70° C., and the reaction time is 8 hours.
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