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Preparation method of antibacterial non-woven cloth and antibacterial non-woven cloth

A technology of non-woven fabrics and polylactic acid fibers, applied in the field of non-woven fabrics, can solve the problems of polylactic acid fibers with high hardness, insufficient softness, and poor hand feeling of non-woven fabrics, and achieve antibacterial performance improvement, content reduction, and hydrophilic sex good effect

Active Publication Date: 2018-10-16
阳光卫生医疗科技江阴有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The polylactic acid fiber in the prior art has antibacterial effect, but the hardness of the polylactic acid fiber is relatively large, and the softness is insufficient, and it is used as a blended fiber of a nonwoven fabric, which will make the hand feeling of the nonwoven fabric worse, and achieve a certain antibacterial effect. performance, it is necessary to control the amount of polylactic acid used in nonwovens, but the cost of polylactic acid fibers is relatively high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The preparation method of embodiment 1 antibacterial nonwovens comprises the following steps:

[0028] S1, hydrophilic modification of polylactic acid fibers in a mixed solution of water and lipase to obtain hydrophilic polylactic acid fibers;

[0029] S2: The hydrophilic polylactic acid fiber is immersed in a grafting treatment solution containing nanocrystalline cellulose, an esterification catalyst, and an ionic liquid for grafting reaction to obtain a cellulose-grafted polylactic acid fiber;

[0030] S3: Laying cellulose-grafted lactic acid fibers into a single component, fiber web, or blending cellulose-grafted lactic acid fibers with second fibers to form a mixed fiber web, spunlace, washing and drying, to obtain antibacterial non-toxic Finished woven cloth.

[0031] The lipase in S1 is porcine pancreatic lipase L3126, and the composition of S1 mixed solution comprises lipase and disodium hydrogen phosphate-potassium dihydrogen phosphate buffer solution, and the ...

Embodiment 2

[0037] Embodiment 2 is based on Example 1, the difference is that the lipase in S1 is porcine pancreatic lipase L3126, and the composition of S1 mixed solution comprises lipase and disodium hydrogen phosphate-potassium dihydrogen phosphate buffer solution, disodium hydrogen phosphate-phosphoric acid The pH value of potassium dihydrogen buffer solution is 7.7; the technological conditions of S1 hydrophilic modification are: reaction temperature 43°C, reaction time 12h, lipase L3126 concentration 0.3g / L.

Embodiment 3

[0039] The difference between Example 3 and Example 2 is that the ionic liquid is 1-butyl-3-imidazole carboxylate.

[0040] The weight percentage of nanocrystalline cellulose in the grafting treatment liquid is 2%, and the weight percentage of the esterification catalyst in the grafting treatment liquid is 1%.

[0041] The technological conditions of the grafting reaction in S2 are: the reaction temperature is 70° C., and the reaction time is 8 hours.

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PUM

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Abstract

The invention discloses a preparation method of antibacterial non-woven cloth. The preparation method comprises the following steps that S1, hydrophilic modification is carried out on a polylactic acid fiber under a mixed solution of water and lipase to obtain a hydrophilic polylactic acid fiber; S2, the hydrophilic polylactic acid fiber is soaked into a grafting treating fluid containing nano-crystal cellulose, esterification catalyst and ionic liquid for grafting reaction to obtain a cellulose grafting polylactic acid fiber; S3, lapping is carried out on the cellulose grafting polylactic acid fiber to obtain a single component and a fiber web, or blend lapping is carried out on the cellulose grafting polylactic acid fiber and a second fiber to obtain a mixed fiber web, and spunlace, cleaning and drying are carried out to obtain an antibacterial non-woven cloth finished product. The obtained polylactic acid fiber has good flexibility and hydrophilia, the antibacterial property is further improved, and based on the same antibacterial effect, the content of the polylactic acid fiber used in a blend fiber of the non-woven cloth can be reduced properly. The invention further disclosesthe antibacterial non-woven cloth and application thereof.

Description

technical field [0001] The invention belongs to the technical field of nonwoven fabrics, and in particular relates to a preparation method of an antibacterial nonwoven fabric and the antibacterial nonwoven fabric. Background technique [0002] Spunlaced nonwovens spray high-pressure fine water onto one or more layers of fiber webs. Due to its wide range of raw materials, soft and fluffy feel, appropriate strength, no warp and weft, convenient cutting and sewing, and light weight and easy shaping, it is Widely used in beauty, hygiene and medical fields. [0003] There are three types of ecological antibacterial nonwovens in the prior art. The first is to use antibacterial fibers as one of the nonwoven fibers or blended fibers, the second is to use ecological antibacterial agents as finishing agents grafted, and the third is the above-mentioned A combination of the first and the second. The first natural antibacterial fibers include hemp fiber, bamboo fiber, tea fiber, chiti...

Claims

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Application Information

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IPC IPC(8): D04H1/4382D04H1/435D06M11/71D06M15/05D06M16/00D06M101/32
CPCD04H1/435D04H1/4382D06M11/71D06M15/05D06M16/003D06M2101/32
Inventor 孙瑜孙一帆曹秀明
Owner 阳光卫生医疗科技江阴有限公司
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