Silicon carbide oxidation method based on two-step microwave plasma oxidation
A microwave plasma and oxygen plasma technology, applied in semiconductor/solid-state device manufacturing, electrical components, circuits, etc., can solve the problems of long oxidation time, unsatisfactory interface quality, low oxidation efficiency, etc., to reduce carbon residue, reduce Electronic defects, the effect of improving surface roughness
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[0047] The microwave input power of the microwave plasma generating device is set to 1000w, and the adjustable range of the microwave frequency for exciting the microwave plasma is 2.4-2.5GHz. At air pressure 100mTorr, H 2 :O 2=1:1 environment, the initial temperature of the sample stage is set to 100°C, the plasma temperature rises at a rate of 1°C / s, and reaches 350°C for low-temperature oxidation, and the plasma discharge time is 400s; then, change the heating rate to 0.5°C / s until the set microwave plasma oxidation temperature is 800°C, change the gas to pure oxygen, change the air pressure to 800mTorr, and set the plasma discharge time to 800s for high-temperature oxidation. The thickness of the oxide layer is about 30nm, and the oxidation is completed Finally, change the pure oxygen to pure nitrogen, and cool down in a nitrogen atmosphere.
[0048] Depend on image 3 It can be seen that adopting the plasma oxidation process of the present invention forms SiC / SiO 2 Th...
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