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Super-smooth glass optical lens multilevel ion polishing method

A glass lens, ion polishing technology, applied in the field of ultra-smooth glass lens polishing, can solve the adverse effects of lens quality, surface abnormalities, lens quality degradation and other problems, to reduce the main pollutants and defects, reduce local scattering abnormalities, improve the surface quality effect

Active Publication Date: 2018-11-06
HUAZHONG PHOTOELECTRIC TECH INST (CHINA SHIPBUILDING IND CORP THE NO 717 INST)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage of classical polishing is that the subsurface damage layer formed during the polishing process is hidden under the surface of the glass lens, and there are residual gas molecules, nitrides, oxides and other pollutants and submicron defects in the subsurface damage layer. Most of the pollutants and defects exist in the Bielby layer (Bielby layer) in the subsurface damage layer. The thickness of the Bielby layer formed after classical polishing is generally 0.1 to 1 micron
For example: Ar ion bombardment with too high energy can lead to migration and aggregation of Ar atoms after implantation and infiltration, and then form bulging bubbles under the surface layer; during long-term Ar ion bombardment, the incident angles of different regions of the substrate and ion beams are inconsistent. can lead to uneven etching
To sum up, on the one hand, ion beam etching or bombardment removes some pollutants on the surface of the substrate, which helps to improve the bonding force of the film layer when coating the substrate surface. On the other hand, inappropriate ion etching or bombardment Causes new defects to form which can adversely affect final lens quality
[0005] Studies have shown that for ultra-smooth optical components, low surface roughness and low surface defects are the two core indicators of ultra-smooth surfaces. The increase in surface roughness will directly lead to an increase in the scattering loss of the optical surface, and the defects will directly lead to local surface defects. Abnormal, the optical performance changes suddenly at the location of the defect, resulting in a decrease in the quality of the lens

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0022] Ultra-smooth (surface roughness rms=0.11nm) fused silica glass lens surface multi-stage ion polishing method, the entire ion beam polishing is divided into 5 levels, the specific steps are as follows:

[0023] (1) Ultra-smooth glass lens precision cleaning: remove oil, dust and other pollutants remaining on the surface of the substrate to make the substrate clean;

[0024] (2) High-energy ion beam etching to remove the Bierbay layer (first-stage ion beam polishing): place the precisely cleaned fused silica glass lens in a vacuum chamber equipped with a divergent radio frequency ion source, and evacuate to the pressure of the vacuum chamber P=4×10 -4 Pa, incoming flow F 1 = Ar gas of 10sccm, add RF excitation power, start the ion source, adjust the ion beam energy BV 1 =500eV, beam current BI 1 =50mA, etching rate is 0.08nm / s, etching depth D 1 =100nm, etching time T 1 =D 1 / V 1 = 1250s;

[0025] (3) Second-stage ion beam polishing: After the first-stage ion beam...

Embodiment 2

[0031] Ultra-smooth (surface roughness rms=0.11nm) Schott Zedruo glass-ceramic lens surface multi-level ion polishing method, the entire ion beam polishing is divided into 3 levels, the specific steps are as follows:

[0032] (1) Ultra-smooth glass lens is precisely cleaned to remove residual oil, dust and other pollutants on the surface of the substrate to make the substrate clean;

[0033] (2) High-energy ion beam etching to remove the Bierbay layer (first-stage ion beam polishing): place the precisely cleaned fused silica glass lens in a vacuum chamber equipped with a divergent radio frequency ion source, and evacuate to the pressure of the vacuum chamber P=4×10 -4 Pa, incoming flow F 1 = Ar gas of 12sccm, add RF excitation power, start the ion source, adjust the ion beam energy BV 1 =500eV, beam current BI 1 =50mA, etching rate is 0.1nm / s, etching depth D 1 =120nm, etching time T 1 =D 1 / V 1 =1200S;

[0034] (3) Second-stage ion beam polishing: After the first-stag...

Embodiment 3

[0038] Ultra-smooth (surface roughness rms=0.3nm) K9 glass lens surface multi-level ion polishing method, the entire ion beam polishing is divided into 100 levels, the specific steps are as follows:

[0039] (1) Ultra-smooth glass lens precision cleaning: remove oil, dust and other pollutants remaining on the surface of the substrate to make the substrate clean;

[0040] (2) High-energy ion beam etching to remove the Bierbay layer (first-stage ion beam polishing): place the precisely cleaned fused silica glass lens in a vacuum chamber equipped with a divergent radio frequency ion source, and evacuate to the pressure of the vacuum chamber P=4×10 -4 Pa, incoming flow F 1 = 20sccm of Ar gas, add RF excitation power, start the ion source, adjust the ion beam energy BV 1 =600eV, beam current BI 1 =50mA, etching rate is 0.15nm / s, etching depth D 1 =150nm, etching time T 1 =D 1 / V 1 =2000S;

[0041] (3) Second-stage ion beam polishing: After the first-stage ion beam polishing...

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Abstract

The invention belongs to the technical field of super-smooth glass optical lens polishing, and particularly relates to a super-smooth glass optical lens multilevel ion polishing method. High-energy inert gas ion (such as Ar+ and Xe+) beams are adopted for rapidly etching and removing a Beilby layer in a sub-surface damage layer of a super-smooth surface, and the surface roughness of the super-smooth surface of glass and oxygen losses of oxide components are inevitably increased after ion beam rapid etching; and in order to lower the roughness of the super-smooth surface after the super-smoothsurface is etched by the high-energy ion beams, the multilevel ion polishing method is adopted, by reducing energy of the ion beams, increasing the concentration of oxygen irons in the ion beams gradually and decreasing the concentration of inert gas ions in the ion beams gradually at the same time, the roughness is lowered, the oxide components of which oxygen is lost are oxidized again, finallythe Beilby layer is removed successfully under the condition that the roughness of the super-smooth surface is changed slightly, main pollutants and defects in the damage layer of the super-smooth surface of the super-smooth surface are greatly reduced, and the optical performance of optical elements is effectively improved.

Description

technical field [0001] The invention belongs to the technical field of ultra-smooth glass lens polishing, and in particular relates to a multi-stage ion polishing method for an ultra-smooth glass lens. Background technique [0002] Ultra-smooth glass lenses (rms≤0.3nm) have important and extensive applications in strong laser systems, laser gyroscopes, extreme ultraviolet lithography, and gravitational wave detection systems. At present, the methods for manufacturing such ultra-smooth glass lenses include traditional classical polishing method, float polishing method, ion beam polishing method, etc. Among them, the ultra-smooth glass surface obtained by traditional classical polishing method has high cost performance, so , has been widely used in industrial production. The disadvantage of classical polishing is that the subsurface damage layer formed during the polishing process is hidden under the surface of the glass lens, and there are residual gas molecules, nitrides, o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B24B1/00
CPCB24B1/002
Inventor 李钱陶李定王潺金天义熊长新
Owner HUAZHONG PHOTOELECTRIC TECH INST (CHINA SHIPBUILDING IND CORP THE NO 717 INST)