Preparation method for multilayer composite photosensitive artificial skin sensor
A technology of artificial skin and multi-layer composite, applied in the fields of medical formula, medical science, prosthesis, etc., can solve the problems of lack of natural skin tactile feeling and signal transmission function, physical and mechanical properties that do not meet the use requirements, complex production, etc. Achieving good external force response, improving poor mechanical properties, and less environmental pollution
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Embodiment 1
[0029] A method for preparing a multilayer composite photosensitive artificial skin sensor, comprising the following preparation steps:
[0030] Step 1): adding the graphene after grinding and pulverizing into the HI / HAC solution for dispersion, preparing a graphene HI / HAC solution with a concentration of 0.1 g / ml, and freeze-drying the graphene HI / HAC solution, wherein The molar concentrations of HI and HAC in the HI / HAC solution are both 0.1mol / L;
[0031] Step 2): put the freeze-dried sample into toluene and sonicate for 1 hour to obtain a broken graphene sponge, place the graphene sponge in a centrifuge with a speed of 3000rmp, and wash it twice with deionized water, each time Wash for 2 minutes;
[0032] Step 4): Centrifuge the mixed solution A after the oil bath reaction in step 3), take the precipitate, and use absolute ethanol and deionized water to wash centrifugally respectively to obtain the graphene oxide-silver nanocomposite material, and the graphene oxide - ad...
Embodiment 2
[0040] A method for preparing a multilayer composite photosensitive artificial skin sensor, comprising the following preparation steps:
[0041] Step 1): adding the graphene after grinding and pulverizing into the HI / HAC solution for dispersion, preparing a graphene HI / HAC solution with a concentration of 0.3g / ml, and freeze-drying the graphene HI / HAC solution, wherein The molar concentrations of HI and HAC in the HI / HAC solution are both 0.5mol / L;
[0042] Step 2): Put the freeze-dried sample into toluene and sonicate for 2.5 hours to obtain a broken graphene sponge, place the graphene sponge in a centrifuge at a speed of 5500rmp, and centrifugally wash it with deionized water 4 times. Wash for 4 minutes;
[0043] Step 4): Centrifuge the mixed solution A after the oil bath reaction in step 3), take the precipitate, and use absolute ethanol and deionized water to wash centrifugally respectively to obtain the graphene oxide-silver nanocomposite material, and the graphene oxide...
Embodiment 3
[0051] A method for preparing a multilayer composite photosensitive artificial skin sensor, comprising the following preparation steps:
[0052] Step 1): adding the graphene after grinding and pulverizing into the HI / HAC solution for dispersion, preparing a graphene HI / HAC solution with a concentration of 0.5g / ml, and freeze-drying the graphene HI / HAC solution, wherein The molar concentrations of HI and HAC in the HI / HAC solution are both 1mol / L;
[0053] Step 2): Put the freeze-dried sample into toluene for 4 hours of supersonication to obtain a broken graphene sponge, place the graphene sponge in a centrifuge with a rotation speed of 8000rmp, and centrifugally wash it with deionized water 5 times, each time Wash for 5 minutes;
[0054] Step 4): Centrifuge the mixed solution A after the oil bath reaction in step 3), take the precipitate, and use absolute ethanol and deionized water to wash centrifugally respectively to obtain the graphene oxide-silver nanocomposite material,...
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