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A nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface and its preparation method and application

A hydroxyl functional group, nanofiber technology, applied in fiber treatment, fiber chemical characteristics, preparations for skin care, etc., can solve problems such as lack of moisturizing function, affecting the activity of active ingredients, skin allergies, etc.

Active Publication Date: 2021-04-20
慧丝纳米科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the adhesive material may cause skin allergies, and the method of chemical modification will affect the activity of the active ingredients and increase the cost. For example, Chinese patent CN104114057A discloses a mask impregnated with liquid cosmetic preparations, and the nanofiber layer is bonded To the nonwoven fabric layer, the adhesive materials used include: acrylic, polyurethane, polyester and silicone
Although these viscous materials are inherently sticky, they do not have a moisturizing function

Method used

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  • A nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface and its preparation method and application
  • A nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface and its preparation method and application
  • A nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface and its preparation method and application

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preparation example Construction

[0024] The invention provides a method for preparing a nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface, comprising the following steps:

[0025] (1) mixing a solute comprising glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin and sodium pyrrolidone carboxylate with a solvent to obtain a spinning solution;

[0026] (2) the spinning liquid electrospinning that described step (1) obtains is to the one side of mask base material, forms sticky nanofiber layer on described mask base material surface;

[0027] (3) The surface of the viscous nanofiber layer obtained in the step (2) is pasted with a protective layer to obtain a nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface.

[0028] In the invention, the solute including glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin and sodium pyrrolidone carboxylate is mixed with a solvent to obtain a spinning solution. In the present invention, the ...

Embodiment 1

[0051] Glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin, sodium pyrrolidone carboxylate and a solvent are mixed to obtain a spinning solution, and the solute in the spinning solution includes the following components by weight fraction: glycerin 15%, Hyaluronic acid 30%, polyethylene oxide 15%, urea 15%, allantoin 10%, sodium pyrrolidone carboxylate 15%.

[0052] Spinning liquid is on mask substrate (spun-bonded non-woven fabric, and film resistance is 107Ω / sq, and gram weight is 10g / m 2 ) for electrospinning, the electrospinning voltage is 20kV, the electrospinning time is 0.5h, the distance between the spinneret and the mask substrate is 18cm, the moving speed of the mask substrate is 0.1m / min, and the injection speed At 1 mL / min, a viscous nanofiber layer of 50 μm was obtained. The resulting viscous nanofibrous layer was observed under a microscope, and the results were as follows figure 2 ,Depend on figure 2 It can be seen that the sticky nanofiber layer...

Embodiment 2

[0062] Glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin, sodium pyrrolidone carboxylate and a solvent are mixed to obtain a spinning solution, and the solute in the spinning solution includes the following components by weight fraction: glycerin 15%, Hyaluronic acid 10%, polyethylene oxide 15%, urea 15%, allantoin 10%, sodium pyrrolidone carboxylate 15%, hydrolyzed collagen 20%.

[0063] Spinning liquid is on mask substrate (spun-bonded non-woven fabric, and film resistance is 100Ω / sq, and gram weight is 12g / m 2 ) carries out electrospinning on one side, the electrospinning voltage is 100kV, the time of electrospinning is 5, the distance between the spinneret and the mask base material is 10cm, the moving speed of the mask base material is 2.0m / min, and the injection speed is 0.1 mL / min to obtain a viscous nanofiber layer of 50 μm.

[0064] The sticky nanofiber layer is bonded to the pearl film to obtain a nanofiber moisturizing mask with sticky hydroxyl functio...

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Abstract

The invention provides a preparation method of a nanofiber moisturizing mask with viscous hydroxyl functional groups on the surface, which belongs to the field of skin care products. Mix glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin, sodium pyrrolidone carboxylate, and a solvent to obtain a spinning solution and perform electrospinning on one side of the mask substrate to obtain a viscous nanofiber layer. The protective layer is attached and you get a nanofiber moisturizing mask. In the present invention, the spinning liquid is skillfully mixed with glycerin, hyaluronic acid, polyethylene oxide, urea, allantoin, and sodium pyrrolidone carboxylate. After the glycerin is electrospun into nanofibers, its surface area is greatly increased, and the hydroxyl functional group fully contacts the mask substrate, which is sticky, ensuring the bonding performance between the viscous nanofibers and the mask substrate.

Description

technical field [0001] The invention relates to the technical field of skin care products, in particular to a nanofiber moisturizing facial mask with viscous hydroxyl functional groups on the surface, a preparation method and application thereof. Background technique [0002] Ordinary nanofiber spinning facial mask comprises nanofiber layer and facial mask substrate layer, and wherein nanofiber layer peels off easily with facial mask substrate layer, and the solution in the prior art is to add one layer of macromolecule material adhesive in the middle of two layers, Or use chemical methods to make a chemical reaction between the two layers to increase the adhesion. However, the adhesive material may cause skin allergies, and the method of chemical modification will affect the activity of the active ingredients and increase the cost. For example, Chinese patent CN104114057A discloses a mask impregnated with liquid cosmetic preparations, and the nanofiber layer is bonded To t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/34A61K8/73A61K8/86A61K8/42A61K8/49A61K8/02A61K8/65A61Q19/00D01D5/00
CPCA61K8/0212A61K8/345A61K8/42A61K8/4913A61K8/4946A61K8/65A61K8/735A61K8/86A61Q19/00D01D5/003D01D5/0084D01F9/00
Inventor 李明明唐滈宏郭秀娟王钧平
Owner 慧丝纳米科技有限公司
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