A kind of preparation method of high tg copper clad laminate
A copper-clad laminate and epoxy resin technology, applied in the direction of chemical instruments and methods, applications, and other household appliances, to achieve the effects of improving production efficiency, solving cracking boards, and improving stability
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Embodiment 1
[0032] A preparation method of high Tg copper clad laminate, the steps are as follows:
[0033] (1) Preparation of glue solution: according to parts by weight, 8 parts of bisphenol F type epoxy resin, 20 parts of modified anhydride containing naphthalene ring, 20 parts of bisphenol F type brominated epoxy resin, tetraphenol ethane 5 parts of glycidyl ether, 3 parts of polyphenylene ether modified epoxy resin, 30 parts of naphthalene ring type benzoxazine resin, 20 parts of silicon micropowder and 20 parts of toluene are mixed to make glue;
[0034] (2) Use reinforcing material to dip the glue in step (1), and bake to make prepreg; under IPC standard detection, the prepreg reaches: fluidity 5-35%, gelation time 50-150s; prepreg air bubble content is: In the area of 4"*4", the diameter of the bubbles is ≤40μm, the number of bubbles with a diameter of 20-40μm is less than 2, and the number of bubbles with a diameter of 10-20μm is less than 5;
[0035] (3) Take 5 sheets of prep...
Embodiment 2
[0037] A preparation method of high Tg copper clad laminate, the steps are as follows:
[0038] (1) Preparation of glue: according to parts by weight, 9 parts of bisphenol A type epoxy resin, 18 parts of dicyclopentadiene maleic anhydride, 15 parts of bisphenol A type brominated epoxy resin, tetraphenol ethane 8 parts of glycidyl ether, 2 parts of isocyanate modified epoxy resin, 25 parts of bisphenol A benzoxazine resin and 25 parts of acetone are mixed to make glue;
[0039] (2) Use reinforcing material to dip the glue in step (1), and bake to make prepreg; under IPC standard detection, the prepreg reaches: fluidity 5-35%, gelation time 50-150s; prepreg air bubble content is: In the area of 4"*4", the diameter of the bubbles is ≤40μm, the number of bubbles with a diameter of 20-40μm is less than 2, and the number of bubbles with a diameter of 10-20μm is less than 5;
[0040] (3) Take 5 sheets of prepregs and add metal foil on one side of the prepregs. The rough surface of...
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