Preparation technology of self-suspension coated support material

A supporting material and preparation technology, which is applied in the direction of drilling composition, production fluid, wellbore/well parts, etc., can solve the problems of increased construction cost, increased production cost, and high cost, so as to reduce construction cost and improve work efficiency. Efficiency and reduced equipment requirements

Inactive Publication Date: 2019-01-01
CHONGQING CHANGJIANG RIVER MOLDING MATERIAL GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This type of product can indeed achieve semi-suspension in water and reduce the settling rate of proppant in water, but because the apparent density must be greatly reduced, its production cost will be greatly increased, and the performance of proppant, such as crushing, acid solubility, and diversion and other performance will be significantly reduced
However, the low production efficiency and high cost of resin pellets also limit its popularization and use.
Moreover, although the above-mentioned proppant can realize self-suspension in water, the frictional resistance of the carrier fluid has been greatly improved, so that a higher pump pressure is required to pump the proppant to the corresponding position during construction, which increases the construction cost.

Method used

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  • Preparation technology of self-suspension coated support material
  • Preparation technology of self-suspension coated support material
  • Preparation technology of self-suspension coated support material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] Take the apparent density as 1.05g / cm 3 100 parts of ceramsite with a particle size of 20 / 40, heated to 180-190°C, poured the heated ceramsite into a bowl-shaped mixing casserole, then added 2 parts of epoxy resin and stirred; the temperature dropped to 150-160°C, added 0.2 parts of modified aromatic amine curing agent (T31) and stir; the temperature drops to 140-150 ° C, then add 0.3 parts of drag reducer and mix; the temperature drops to 80-90 ° C, add 2 parts of propylene glycol and 0.02 parts of dilaurel Stir with dibutyltin acid; when the temperature drops to 70-80°C, add 0.2 parts of ethylenediamine and stir; when the temperature drops to 60-70°C, add 0.8 parts of toluene diisocyanate and stir; Resist mixed; the temperature dropped to 40-50 ℃ out of the pot. Epoxy resin and modified aromatic amine curing agent form an inner resin film, and the inner resin film is an epoxy resin film; glycerol, dibutyltin dilaurate, diethylenetriamine and toluene diisocyanate form...

Embodiment 2

[0041] Take the apparent density as 1.65g / cm 3 100 parts of ceramsite with a particle size of 30 / 50, heated to 220-230°C, poured the heated ceramsite into a bowl-shaped mixing casserole, then added 3 parts of phenolic resin and stirred; when the temperature dropped to 190-200°C, added 0.6 1 part of hexamethylenetetramine and stir; the temperature drops to 180-190°C, and then 0.6 parts of drag reducer are added and mixed; When the temperature drops to 100-110°C, add 0.2 parts of triethylamine and stir; when the temperature drops to 90-100°C, add 1 part of methylene diphenyl diisocyanate and stir; when the temperature drops to 70-80°C, add 0.6 parts of drag reduction The agent is mixed; the temperature is lowered to 60-70 ℃ and the pot is taken out.

Embodiment 3

[0043] Take the apparent density as 2.05g / cm 3 100 parts of ceramsite with a particle size of 40 / 70, heated to 80-90°C, poured the heated ceramsite into a bowl-shaped mixing casserole, then added 2 parts of ethylene glycol and 0.02 parts of tributyltin and stirred; the temperature dropped to 70 -80°C, add 0.6 parts of isophorone diisocyanate and stir; when the temperature drops to 60-70°C, add 0.7 parts of drag reducer and mix; when the temperature drops to 50-60°C, add 4 parts of glycerol and 0.02 parts of Stir with lead isooctanoate; when the temperature drops to 40-50°C, add 0.2 parts of triethylamine and stir; when the temperature drops to 35-45°C, add 1 part of methylene diphenyl diisocyanate and stir; when the temperature drops to 30-40°C, Then add 0.8 parts of drag reducer and mix; the temperature is lowered to 30-35°C and taken out of the pot.

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Abstract

The invention belongs to the technical field of production of fluid ores of petroleum, natural gas, shale gas and the like, and particularly discloses a preparation technology of a self-suspension coated support material. The preparation technology comprises the following steps: (1) heating aggregate to the temperature of 80 to 230 DEG C, and stirring and mixing the heated aggregate; (2) cooling to the temperature of 75 to 200 DEG C, adding inner resin and a curing agent of the inner resin, and stirring, thus forming an inner coating layer; (3) cooling to the temperature of 65 to 190 DEG C, adding a drag reducer, and stirring; (4) cooling to the temperature of 55 to 130 DEG C, adding a catalyst, outer resin, an amine additive and a curing agent of the outer resin, and stirring, thus forming an outer coating layer; (5) cooling to the temperature of 40 to 80 DEG C, adding a blocking agent, and stirring; (6) cooling to the temperature of 30 to 70 DEG C, discharging out of a pot, and controlling the apparent density of a low-density support agent within the range of 1.05 to 2.60g/cm<3>. The self-suspension coated support material prepared by the preparation technology has the advantages that the flow guide property is good, the self-suspension property is good, and the friction drag is low.

Description

technical field [0001] The invention belongs to the technical field of fluid mineral exploitation such as oil, natural gas and shale gas, and in particular relates to a preparation process of a self-suspension film-coated support material. Background technique [0002] Hydraulic fracturing technology has been relatively mature at home and abroad. Petroleum fracturing proppant is one of the essential items in the fracturing process. Its performance will directly affect the effect of hydraulic fracturing. The apparent density is the key to evaluate the performance of proppant. One of the important indicators, the lower the apparent density, the lower its relative density relative to the fracturing fluid. When the proppant is mixed with the fracturing carrier fluid, the lower the apparent density, the easier it is to suspend in the fracturing fluid, thereby greatly reducing sedimentation rate. Push the pump farther during the pumping process. The high pumping pressure pumps t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/80
CPCC09K8/805
Inventor 熊帆熊鹰王正力陈秋庆
Owner CHONGQING CHANGJIANG RIVER MOLDING MATERIAL GRP
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