Antifouling paint and preparation method thereof
A technology of antifouling coatings and raw materials, applied in the field of coatings, can solve the problems of excessive release of copper ions, low efficiency, single antifouling performance, etc., and achieve the effect of keeping smooth and pollution-free, increasing residence time, and reducing microbial pollution
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Embodiment 1
[0027] An antifouling coating is prepared from the following raw materials in parts by weight: 20 parts of modified acrylic resin, 1 part of capsaicin derivative, 3 parts of copper ion slow-release agent, 5 parts of rosin, 15 parts of filler, 0.5 parts of antioxidant 100 parts and solvent;
[0028] The copper ion sustained-release agent is prepared by the following method: 1mmol of CuSO 4 ·5H 2 O and 8 mmol of dimethylaminoethyl methacrylate were dissolved in 200ml of methanol, and after stirring at room temperature for 12 h, the solvent methanol was removed, and the remaining solid was washed with acetone for 3 times to remove excess dimethylaminoethyl methacrylate, and depressurized at room temperature Dry for 12h to obtain copper ion sustained-release agent;
[0029] 1 mmol CuSO 4 • 5H 2 O and 8mmol of dimethylaminoethyl methacrylate were dissolved in 200ml of methanol and reacted after mixing. The color of the solution changed from light blue to dark green rapidly, and...
Embodiment 2
[0043] An antifouling coating is prepared from the following raw materials in parts by weight: 35 parts of modified acrylic resin, 3 parts of capsaicin derivatives, 8 parts of copper ion slow-release agent, 10 parts of rosin, 25 parts of filler, 1 part of antioxidant 200 parts and solvent;
[0044] The copper ion sustained-release agent is prepared by the following method: 1mmol of CuSO 4 ·5H 2 O and 8 mmol of dimethylaminoethyl methacrylate were dissolved in 200ml of methanol, and after stirring at room temperature for 12 hours, the solvent methanol was removed, and the remaining solid was washed 5 times with acetone to remove excess dimethylaminoethyl methacrylate, and depressurized at room temperature Dry for 24h to obtain copper ion sustained-release agent;
[0045] The modified acrylic resin is prepared from the following steps:
[0046] (1) Weigh methyl methacrylate, butyl acrylate, vinyltriethoxysilane, xylene and butyl acetate in a beaker according to the mass ratio...
Embodiment 3
[0058] An antifouling coating is prepared from the following raw materials in parts by weight: 30 parts of modified acrylic resin, 2 parts of capsaicin derivatives, 5 parts of copper ion slow-release agent, 8 parts of rosin, 20 parts of filler, 0.8 parts of antioxidant 150 parts and solvent;
[0059] The copper ion sustained-release agent is prepared by the following method: 1mmol of CuSO 4 ·5H 2 O and 8 mmol of dimethylaminoethyl methacrylate were dissolved in 200ml of methanol, and after stirring at room temperature for 12 hours, the solvent methanol was removed, and the remaining solid was washed 4 times with acetone to remove excess dimethylaminoethyl methacrylate, and depressurized at room temperature Dry for 18h to obtain copper ion sustained-release agent;
[0060] The modified acrylic resin is prepared from the following steps:
[0061] (1) Weigh methyl methacrylate, butyl acrylate, vinyltriethoxysilane, xylene and butyl acetate in a beaker according to the mass rat...
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