A kind of high-strength hot air seaweed membrane cloth and preparation method thereof
A high-strength, hot-air technology, used in wet spinning, non-woven fabrics, rayon manufacturing, etc., can solve the problems of easy deformation and low strength, and achieve the effects of not easy to deform, high strength, and good antibacterial properties.
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Embodiment 1
[0021] A preparation method of a high-strength hot-air seaweed membrane cloth, comprising the following steps:
[0022] (1) Sodium alginate is dissolved in water at room temperature, stirred at a high speed to make a 3% sodium alginate aqueous solution by mass, and left to stand for defoaming to obtain a sodium alginate spinning solution;
[0023] (2) The spinning solution left to stand for defoaming is metered and ejected from the spinneret into the first coagulation bath through a metering pump, and drawn by 60%, to obtain as-spun fibers, and the mass fraction of the first coagulation bath is 3%. Calcium chloride aqueous solution, the temperature of the first coagulation bath is 45-50 ℃, and the coagulation time is 1min;
[0024] (3) As-spun fibers are washed with distilled water, and then introduced into the second coagulation bath, drawing 35%. The second coagulation bath is an aqueous solution of calcium hydrogen phosphate with a mass fraction of 0.01%, and the temperatur...
Embodiment 2
[0030] A preparation method of a high-strength hot air seaweed membrane cloth, comprising the following steps:
[0031] (1) dissolving sodium alginate in water at room temperature, stirring at a high speed to make an aqueous solution of sodium alginate with a mass percentage of 2%, and standing for defoaming to obtain a sodium alginate spinning solution;
[0032] (2) The spinning solution left standing for defoaming is metered and ejected from the spinneret to the first coagulation bath through a metering pump, and drawn by 60%, to obtain as-spun fibers, and the mass fraction of the first coagulation bath is 2%. Calcium chloride aqueous solution, the temperature of the first coagulation bath is 45-50 ℃, and the coagulation time is 2min;
[0033] (3) As-spun fibers are washed with distilled water, then introduced into the second coagulation bath, and stretched by 40%. The second coagulation bath is an aqueous solution of calcium hydrogen phosphate with a mass fraction of 0.02%,...
Embodiment 3
[0039]A preparation method of a high-strength hot-air seaweed membrane cloth, comprising the following steps:
[0040] (1) Sodium alginate is dissolved in water at room temperature, stirred at a high speed to make a 4% sodium alginate aqueous solution by mass, and left to stand for defoaming to obtain a sodium alginate spinning solution;
[0041] (2) The spinning solution left standing for defoaming is metered and ejected from the spinneret to the first coagulation bath through a metering pump, and drafted by 80% to obtain as-spun fibers. The mass fraction of the first coagulation bath is 3%. Calcium chloride aqueous solution, the temperature of the first coagulation bath is 45-50 ℃, and the coagulation time is 1min;
[0042] (3) The as-spun fiber is washed with distilled water, soaked for 25min with the ammonium citrate solution of dicalcium phosphate of 0.1mmol / L, then introduced into the second coagulation bath, stretched by 30%, and the second coagulation bath is the mass ...
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