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Method for improving extraction rate of cereal starch by extrusion combined alkali method

A technology of extrusion and puffing and extraction rate, which is applied in the field of food industry, can solve the cumbersome; Chinese invention patent (application announcement, not suitable for mass production, low starch extraction rate, etc., to achieve shortened extraction time, shortened soaking time, The effect of increasing the extraction rate

Inactive Publication Date: 2019-02-12
SHENYANG NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method uses lye twice when extracting starch, and the processing process is more loaded down with trivial details; Chinese invention patent (application publication number: CN 1974602 A, application publication date: 2007.06.06) discloses extracting oat starch, oat protein powder from oat. Production technology, the steps include rolling oats to obtain oat kernels, soaking oat kernels, refining, centrifuging to obtain oat starch and oat protein liquid; purifying, drying and pulverizing to obtain oat starch, and the present invention can extract two products at the same time by using one process , but enzymes are used in the starch purification process, the cost of enzymes is high, and it is not suitable for mass production in industry; Chinese invention patent (application publication number: CN 104817644 A, application publication date: 2015.08.05) discloses a rice starch The preparation method involves five steps in total to obtain rice starch through milling, enzyme reaction, centrifugal washing, supernatant removal, and drying. Although the preparation process is simple and easy to operate, the ground rice flour is soaked in enzyme solution. During the soaking process, the temperature is about 55°C, and lye needs to be added to control the pH, and the starch extraction rate is low

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  • Method for improving extraction rate of cereal starch by extrusion combined alkali method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Weigh 20kg of buckwheat, clean and remove impurities and then crush and remove the husks. The buckwheat after removing the husks is pulverized into 60-mesh powder with a pulverizer, and loaded into the hopper of the extruder. 35°C, 35°C, 45°C, 45°C, 50°C, the screw speed is 300rpm, the moisture content of the material is 45%, the diameter of the material outlet hole of the extruder die is 3mm, the extruded material is mixed with 0.08% hydrogen The sodium oxide solution was mixed, the ratio of material to liquid was 1:4, left standing for 8 hours, the supernatant was poured out, the lower mixed solution was centrifuged at 4000 r / min for 20 min, and the upper layer was removed after centrifugation to obtain crude starch milk; L hydrochloric acid was stirred evenly, washed by centrifugation at 5000r / min for 10min, then washed with water for 3 times to obtain pure starch milk, and then dried in an oven at 50°C for 24h to obtain the finished buckwheat starch, with a starch ex...

Embodiment 2

[0031] Weigh 20kg of rice, crush the rice into powder with a pulverizer after pretreatment, put it into the hopper of the extruder, and set the temperature of the six zones of the extruder to be 35°C, 40°C, 40°C, 50°C, 50°C, respectively. ℃, 60℃, the screw speed is 400rpm, the water content of the material is 40%, the diameter of the material outlet hole of the extruder die head is 3mm, the extruded material is mixed with 0.06% sodium hydroxide solution, and the material-liquid ratio is 1: 4. Let stand for 10h, pour off the supernatant, centrifuge the lower layer mixture at 5000r / min for 15min, remove the upper layer after centrifugation to obtain crude starch milk; add 0.5mol / L hydrochloric acid to the crude starch milk, stir evenly, and centrifuge once at 4000r / min, The time was 20 minutes, then washed with water for 3 times to obtain pure starch milk, and then dried in an oven at 50° C. for 24 hours to obtain the finished rice starch, and the starch extraction rate was 84%. ...

Embodiment 3

[0033] Weigh 30kg of buckwheat, clean and remove impurities and then crush and remove the husks. The buckwheat after removing the husks is pulverized into a powder of more than 80 meshes with a pulverizer, and is loaded into the hopper of the extruder. The temperature of the six zones of the extruder is set to 35 ℃, 35℃, 40℃, 40℃, 50℃, 60℃, the screw speed is 250rpm, the moisture content of the material is 40%, the diameter of the material outlet hole of the extruder die is 3mm, and the extruded material is mixed with 0.1 % sodium hydroxide solution was mixed, the ratio of material to liquid was 1:3, left standing for 10h, the supernatant was poured out, the lower mixed liquid was centrifuged at 4000r / min for 20min, and the supernatant liquid was removed after centrifugation to obtain crude starch milk; crude starch milk was added with 0.5 mol / L hydrochloric acid was stirred evenly, centrifuged and washed at 5000r / min for 10min, then washed with water for 3 times to obtain pure...

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Abstract

The invention provides a method for improving the extraction rate of cereal starch by an extrusion combined alkali method. The extraction method comprises the following steps: crushing raw materials after removing impurities, and subjecting the crushed cereal to extrusion pretreatment, wherein the temperatures of six sections of a twin-screw extruder are 30 to 40 DEG C in a section I, 35 to 45 DEGC in a section II, 30 to 50 DEG C in a section III, 40 to 55 DEG C in a section IV, 40 to 60 DEG C in a section V, and 45 to 70 DEG C in a section VI, and the number of revolutions is 100 to 400 rpm;soaking the extruded cereal material in an alkali solution, and centrifuging to obtain crude starch milk; washing the crude starch milk with acid and then washing with tap water to obtain pure starchmilk, and drying to obtain a finished starch product. Compared with the traditional alkali method, the concentration of the alkali solution used in the invention is reduced by 50%, the soaking time is shortened by 20 hours, the starch extraction rate is increased by 25%, the extraction time is greatly shortened, the energy consumption is reduced, the extraction rate of starch is greatly improved,and the production efficiency is significantly improved.

Description

technical field [0001] The invention belongs to the field of food industry, and in particular relates to a method for improving the extraction rate of cereal starch by means of extrusion and puffing synergistically with an alkali method. Background technique [0002] Starch is the main component of green plant fruits, seeds, roots and tubers. Cereals are important agricultural products. About 70% of their dry basis is starch. Cereal starch can be digested, absorbed and decomposed by the human body slowly and stably. The release is slow and will not cause a sudden increase in blood sugar, which is beneficial to human health. In addition, cereal starch has some excellent properties. For example, rice starch granules are between 2-8um, the particle size is uniform, the gelatinized rice starch absorbs water quickly, the texture is very smooth and cream-like, and has a fatty taste, which can as a fat substitute. [0003] Extrusion technology is a modern processing technology th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B30/04
CPCC08B30/042
Inventor 肖志刚段玉敏张权峰杨庆余杨国强付昱东王丽爽王娜
Owner SHENYANG NORMAL UNIV