Preparation method of PTFE/SiO2/Al2O3 porous membrane coated on surface of porous aluminum
A technology of surface coating and PTFE, which is used in devices for coating liquids on surfaces, special surfaces, pre-treated surfaces, etc., can solve the problems of reducing the friction between sound waves and porous aluminum, reducing sound absorption performance, etc. The effect of sound function application, high preparation efficiency and high sound absorption characteristics
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[0033] Example 1
[0034] A porous aluminum surface coated with PTFE / SiO 2 / Al 2 O 3 The preparation method of the porous membrane, the specific steps are as follows:
[0035] (1) PTFE / SiO 2 / Al 2 O 3 Preparation of homogeneous liquid
[0036] Combine PTFE emulsion, KH-560 modified silica sol and Al with a particle size of 1~3μm 2 O 3 Particle mixing, where the volume ratio of PTFE emulsion and KH-560 modified silica sol is 1:0.5, Al 2 O 3 The volume fraction of particles is 40% of the total volume of PTFE emulsion and KH-560 modified silica sol. The PTFE emulsion, KH-560 modified silica sol and Al 2 O 3 The mixture of particles is magnetically stirred for 5 hours to obtain PTFE / SiO 2 / Al 2 O 3 Homogeneous mixture.
[0037] (2) The surface of porous aluminum is roughened
[0038] The porous aluminum with a porosity of 60%, a pore diameter of 0.1mm, and a through-hole structure is etched for 60s in a 0.8mol / L NaOH solution. The corroded porous aluminum is washed with deionized water and ...
Example Embodiment
[0045] Example 2
[0046] A porous aluminum surface coated with PTFE / SiO 2 / Al 2 O 3 The preparation method of the porous membrane, the specific steps are as follows:
[0047] (1) PTFE / SiO 2 / Al 2 O 3 Preparation of homogeneous liquid
[0048] Combine PTFE emulsion, KH-560 modified silica sol and Al with a particle size of 3~5μm 2 O 3 Particle mixing, where the volume ratio of PTFE emulsion and KH-560 modified silica sol is 1:0.55, Al 2 O 3 The volume fraction of particles is 31% of the total volume of PTFE emulsion and KH-560 modified silica sol. The PTFE emulsion, KH-560 modified silica sol and Al 2 O 3 The mixture of particles is magnetically stirred for 4.5h to obtain PTFE / SiO 2 / Al 2 O 3 Homogeneous mixture.
[0049] (2) The surface of porous aluminum is roughened
[0050] Porous aluminum with a porosity of 70%, a pore diameter of 1 mm, and a through-hole structure was etched for 90s in a 0.9mol / L NaOH solution. The corroded porous aluminum was washed with deionized water shaking a...
Example Embodiment
[0057] Example 3
[0058] A porous aluminum surface coated with PTFE / SiO 2 / Al 2 O 3 The preparation method of the porous membrane, the specific steps are as follows:
[0059] (1) PTFE / SiO 2 / Al 2 O 3 Preparation of homogeneous liquid
[0060] Combine PTFE emulsion, KH-560 modified silica sol and Al with a particle size of 5-8μm 2 O 3 Particle mixing, where the volume ratio of PTFE emulsion and KH-560 modified silica sol is 1:0.6, Al 2 O 3 The volume fraction of particles is 23% of the total volume of PTFE emulsion and KH-560 modified silica sol. The PTFE emulsion, KH-560 modified silica sol and Al 2 O 3 The mixture of particles is magnetically stirred for 4 hours to obtain PTFE / SiO 2 / Al 2 O 3 Homogeneous mixture.
[0061] (2) The surface of porous aluminum is roughened
[0062] Porous aluminum with a porosity of 80%, a pore diameter of 2 mm and a through-hole structure was etched for 120s in a 1 mol / L NaOH solution. The corroded porous aluminum was washed by shaking with deionized wat...
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