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Preparation method of sodium humate soap

A technology of sodium humate and sodium humate, applied in the direction of chemical instruments and methods, soap detergent compositions, surface active non-soap compounds and washing compositions, can solve the problem of high material cost, weakened decontamination and bactericidal ability , rough skin and other problems, to achieve the effect of simple preparation method, obvious antibacterial effect and good antibacterial effect

Inactive Publication Date: 2019-04-05
杨鹏熙
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the soaps sold on the market contain high artificial soap bases, which can easily lead to rough skin, peeling, dryness, irritation and other problems after long-term use
Although some vegetable oil soaps can overcome the above problems, their decontamination and bactericidal capabilities are weakened, and the cost of materials is expensive, resulting in high prices.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A preparation method of sodium humate soap, comprising the following steps:

[0018] (1) Ingredients: According to the ratio of 5mL: 5mL: 10mL: 5g, mix coconut oil, palm oil, olive oil and lanolin, stir at 40°C, and sonicate under the condition of ultrasonic power of 300W and ultrasonic frequency of 40KHz 10min, obtain oil phase solution;

[0019] (2) Saponification: According to the volume ratio of 1:2, mix the sodium humate solution with a mass concentration of 3% and the sodium hydroxide solution with a mass concentration of 30%, and stir at 40°C for 20 minutes to obtain a mixed solution; In the state, add the mixed solution into the oil phase solution according to the volume ratio of 3:2 to obtain soap liquid;

[0020] (3) Addition of auxiliary materials: Mix the same mass of sodium chloride, sucrose, citric acid, and white fungus powder to obtain a mixed additive, configure a mixed additive solution with a mass concentration of 3%, and add the mixed additive solut...

Embodiment 2

[0023] A preparation method of sodium humate soap, comprising the following steps:

[0024] (1) Ingredients: According to the ratio of 10mL: 10mL: 15mL: 10g, mix coconut oil, palm oil, olive oil and lanolin, stir at 50°C, and sonicate under the condition of ultrasonic power of 500W and ultrasonic frequency of 40KHz 20min, obtain oil phase solution;

[0025] (2) Saponification: According to the volume ratio of 1:2, mix the sodium humate solution with a mass concentration of 5% and the sodium hydroxide solution with a mass concentration of 30%, and stir at 50°C for 15 minutes to obtain a mixed solution; In the state, add the mixed solution into the oil phase solution according to the volume ratio of 4:3 to obtain soap liquid;

[0026] (3) Addition of auxiliary materials: Mix the same mass of sodium chloride, sucrose, citric acid, and white fungus powder to obtain a mixed additive, configure a mixed additive solution with a mass concentration of 5%, and add the mixed additive so...

Embodiment 3

[0029] A preparation method of sodium humate soap, comprising the following steps:

[0030] (1) Ingredients: According to the ratio of 8mL: 7mL: 12mL: 8.5 g, mix coconut oil, palm oil, olive oil and lanolin, stir at 45°C, and ultrasonicate under the condition of ultrasonic power of 400W and ultrasonic frequency of 40KHz Treat for 15 minutes to obtain an oil phase solution;

[0031] (2) Saponification: According to the volume ratio of 1:2, mix the sodium humate solution with a mass concentration of 4% and the sodium hydroxide solution with a mass concentration of 30%, and stir at 45°C for 18 minutes to obtain a mixed solution; Under the state, add the mixed solution into the oil phase solution according to the volume ratio of 3:2.5 to obtain soap liquid;

[0032] (3) Addition of auxiliary materials: Mix equal amounts of sodium chloride, sucrose, citric acid, and white fungus powder to obtain a mixed additive, configure a mixed additive solution with a mass concentration of 4%,...

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Abstract

Disclosed is a preparation method of a sodium humate soap. The preparation method of the sodium humate soap comprises (1) preparing materials, mixing and then stirring coconut oil, palm oil, olive oiland lanum at 40-50 DEG C, and performing ultrasonic treatment to obtain an oil phase solution; (2) performing saponification to obtain liquid soap; (3) adding in auxiliary materials, mixing sodium chloride, saccharose, citric acid and tremella powder of equal weight to obtain mixed additives, preparing a mixed additive solution with a mass concentration of 3-5%, adding and mixing the mixed additive solution into the liquid soap to obtain an added liquid soap; (4) stirring sodium dodecyl sulfate and glycerol into the added liquid soap, and then injecting the mixture into molds for cold forming. The prepared sodium humate soap is simple in preparation and good in inhibiting effects on Escherichia coli and staphylococcus aureus with a bacteriostatic rate up to 95%.

Description

technical field Background technique [0001] Humic acid is mainly a kind of amorphous polymer natural organic matter formed by plant remains through a series of biological and geochemical processes, and widely exists in lignite, weathered coal, and peat in nature. Since humic acid is a macromolecular organic acid that is insoluble in water, it is usually used as a sodium salt that is easily soluble in water. A large number of studies have shown that sodium humate has many plant physiological activities such as salt resistance, drought resistance, and plant growth regulation, as well as significant pharmacological activities such as anti-virus, anti-inflammatory, and immune regulation. The use of humic acid substances to treat and prevent diseases has a history of more than 500 years. The most popular humic acid peat bath in Europe in the 19th and 20th centuries was used to treat skin diseases, infections and arthritis. The application of humic acid in medical care in my cou...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11D10/04
CPCC11D10/042
Inventor 杨鹏熙
Owner 杨鹏熙