Negative ion coating and preparation method thereof
An anion coating, anion technology, applied in the direction of alkali metal silicate coatings, coatings, etc., can solve the problems of lack of negative ion effect, influence of coating quality, easy agglomeration, etc., to reduce surface polarity, ensure stability, The effect of increasing the specific surface area
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[0039] The invention provides a kind of preparation method of negative ion paint, wherein, comprise the following steps:
[0040] 1) Preparation of modified negative ion material:
[0041] A. Mix methyl methacrylate and silane coupling agent to prepare mixture M1;
[0042] B. Under stirring conditions, add negative ion powder to the mixture M1 and mix to prepare the mixture M2;
[0043] C. Grinding the mixture M2 to obtain a slurry M3;
[0044] D, in nitrogen environment, and under the condition that the first solvent exists, polyvinyl alcohol, slurry M3 and initiator are mixed, and modified negative ion material is obtained;
[0045] 2) Preparation of negative ion paint:
[0046] E. Dispersing silicon dioxide in a second solvent, and then adding a surfactant to it to obtain a silica sol;
[0047] F, silicate and silica sol are mixed to prepare silica gel solution;
[0048] G. Mix silica gel liquid, modified negative ion material, processing aid and water to prepare negat...
Embodiment 1
[0072] 1) Preparation of modified negative ion material: Stir and mix 10 parts by weight of methyl methacrylate and 0.5 parts by weight of silane coupling agent under the condition of 600r / min for 15min to prepare mixture M1; heat in a water bath at 40°C Under certain conditions, add 20 parts by weight of anion powder to 10 parts by weight of mixture M1 and stir and mix for 10 minutes at a stirring rate of 300 r / min to obtain mixture M2; put mixture M2 into a ball mill for ball milling for 2 hours to obtain slurry M3; Under ambient conditions, 5 parts by weight of polyvinyl alcohol and 100 parts by weight of water are placed in a water bath at a temperature of 40°C and mixed; then 0.2 parts by weight of an initiator is added thereto to obtain a mixture M4; the above prepared mixture M4 Add 40 parts by weight of the slurry M3 and stir and mix to obtain a modified negative ion material;
[0073] 2) Preparation of negative ion paint: 10 parts by weight of silicon dioxide are disp...
Embodiment 2
[0075] 1) Preparation of modified anion material: Stir and mix 10 parts by weight of methyl methacrylate and 2 parts by weight of silane coupling agent under the condition of 1000r / min for 15min to prepare mixture M1; heat in a water bath at a temperature of 50°C Under certain conditions, add 30 parts by weight of negative ion powder to 10 parts by weight of mixture M1 and stir and mix for 10 minutes at a stirring rate of 500 r / min to obtain mixture M2; put mixture M2 into a ball mill for ball milling for 5 hours to obtain slurry M3; Under ambient conditions, 10 parts by weight of polyvinyl alcohol and 100 parts by weight of water are placed in a water bath at a temperature of 50° C. and mixed; then 0.6 parts by weight of an initiator is added thereto to obtain a mixture M4; the above prepared mixture M4 Add 70 parts by weight of the slurry M3 and stir and mix to obtain a modified negative ion material;
[0076] 2) Preparation of negative ion paint: 40 parts by weight of silic...
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