Mylia taylori sesquiterpene synthetase MTb and gene sequence thereof
A sesquiterpene synthase, calyx moss technology, applied in genetic engineering, plant genetic improvement, lyase and other directions, can solve the problems of little research on moss plants and rarity of lichenaceae plants.
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Embodiment 1
[0020] Example 1. Cloning and expression of the WQ011 / pESC-LEU-MTb bacterial strain Sesquiterpene synthase gene MT-29066
[0021] Total RNA was extracted from Lily calyx by RNAprep pure Plant Kit. The first-strand cDNA was synthesized using the Clontech SMARTer PCRcDNA Synthesis Kit, the first-strand cDNA was amplified by PCR to synthesize the second-strand cDNA, and then the double-strand DNA was amplified by secondary PCR and used for SMRTbell library construction, and PacBio ISO-Seq was used platform for sequencing.
[0022] According to the MT-29066 gene sequence SEQ ID NO.2 obtained by sequencing, primers were designed to amplify the target gene. The primer sequences are as follows:
[0023] Primer MT-29066-F: 5'CGC GGATCC ATGGGGATCGAGACGAGACC 3' (SEQ ID NO. 3)
[0024] Primer MT-29066-R: 5'CCG CTCGAG TCAGACCTTAAAGCGAATGTTTG 3' (SEQ ID NO. 4)
[0025] Using the cDNA sequence obtained by reverse transcription as a template, the MT-29066 gene sequence was amplified b...
Embodiment 2
[0047] Example 2. Induced fermentation
[0048] (1) The transformant WQ011 / pESC-LEU-MTb was transferred to 50 mL of synthetic medium (with out Leu), 180 r / min, 30° C., and cultured on a shaking table for 30 h.
[0049] (2) At 30h, 10g / L galactose was added to induce expression to 90-120h, and at 36h and 72h, 10g / L ethanol was added as a supplementary carbon source.
[0050] (3) The fermentation broth was extracted with 3 mL of n-hexane for 15 min to detect by GC-MS.
Embodiment 3
[0051] Embodiment 3.GC-MS detects fermentation product
[0052] (1) GC-MS detection method
[0053] Chromatographic column: TG-5MS; Ion source; EI, 70eV; Injection volume: 1uL; Injection temperature: 200°C; Detector temperature: 280°C; Column temperature: 240°C; / min Raise the temperature to 280°C and maintain it for 5min.
[0054] (2) The output was calculated by the external standard method. Accurately prepare 0.02, 0.04, 0.06, 0.08 and 1.0 mg / L standard substances respectively, draw a standard curve with the peak area as the ordinate and the concentration as the abscissa.
[0055] The results show that: if image 3 As shown, the target peak in the GC-MS spectrum is compared with the reference mass spectrum data in the NIST14 database, and it is found that the chromatographic peak of the n-hexane extract of the WQ011 / pESC-LEU-MTb strain fermentation broth at a retention time of 17.73min is Piperaceae orange Solanol (Cubedol), 50mL shake flask output is 0.14mg / L. The chr...
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